Keywords: LOQ، محدودیت مقدار; Palytoxin; Hemolytic assay; Matrix effect; Mytilus galloprovincialisPLTX, palytoxin; LOD, limit of detection; LOQ, limit of quantitation; RSDr, relative standard deviation of repeatability; 42-OH-PLTX, 42-hydroxy-palytoxin; Ost-D, Ostreocin-D; OVTX, ovato
مقالات ISI LOQ، محدودیت مقدار (ترجمه نشده)
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Keywords: LOQ، محدودیت مقدار; E1, estrone; E2, estradiol; T, testosterone; μl, microliter; LOD, limit of detection; LOQ, limit of quantitation; sLOQ, serum limit of quantitation; ELISA, enzyme-linked immunosorbent assay; pg, picogram; ml, milliliter; E3, estriol; P4, progesterone (pre
Keywords: LOQ، محدودیت مقدار; Aflatoxin; Raman spectroscopy; ChemometricsFTIR, Fourier transform infrared spectroscopy; HPLC, high-performance liquid chromatography; LDA, linear discriminant analysis; LOD, limit of detection; LOQ, limit of quantitation; MLR, multiple linear regression
Keywords: LOQ، محدودیت مقدار; formulation; excipients; solubility; glass; interaction; glass dissolution; leachable; silicic acid; surface interactions; neutral pH; EDS, energy-dispersive spectroscopy; FTIR, Fourier transform infrared microscopy; ICP-MS, inductively coupled plasmaâ
Measurement of malondialdehyde as oxidative stress biomarker in goat plasma by HPLC-DAD
Keywords: LOQ، محدودیت مقدار; ACN, acetonitrile; DAD, diode array detection; FMDA, free malondialdehyde; HPLC, high performance liquid chromatography; LOD, limit of detection; LOQ, limit of quantitation; MDA, malondialdehyde; PBMDA, protein-bound malondialdehyde; ROS, reactive oxygen
Survey of perfluoroalkyl acids (PFAAs) and their precursors present in Japanese consumer products
Keywords: LOQ، محدودیت مقدار; PFAAs, Perfluoroalkyl acids; LOQ, limit of quantitation; PFOS, perfluorooctane sulfonic acid; MeFOSE, N-methyl perfluorooctane sulfonamidoethanol; PFCAs, perfluoroalkyl carboxylic acids; PFASs, perfluoroalkyl and polyfluoroalkyl substances; PFOA, perfluor
Salicylic acid and methyljasmonate restore the transcription of caffeine biosynthetic N-methyltransferases from a transcription inhibition noticed during late endosperm maturation in coffee
Keywords: LOQ، محدودیت مقدار; CV, coefficient of variation; LOD, limit of detection; LOQ, limit of quantitation; dw, dry weight; NMT, N-methyltransferase; XMT, xanthosine methyltransferase; MXMT, methylxanthine methyltransferase; DXMT, di-methylxanthine methyltransferase; SA, salicyli
A validated HPLC-FLD method for analysis of intestinal absorption and metabolism of capsaicin and dihydrocapsaicin in the rat
Keywords: LOQ، محدودیت مقدار; RP-HPLC, reverse-phase high performance liquid chromatography; FLD, fluorescence detection; LOD, limit of detection; LOQ, limit of quantitation; TRIS, tris(hydroxymethyl)aminomethane; HPLC–MS, high performance liquid chromatography mass spectrometry; RS,
Enhancement of specificity of aldosterone measurement in human serum and plasma using 2D-LC–MS/MS and comparison with commercial immunoassays
Keywords: LOQ، محدودیت مقدار; 2D-LC–MS/MS, two dimensional liquid chromatography tandem mass spectrometry; LOQ, limit of quantitation; LOD, limit of detection; MRM, multiple reaction monitoring; LLE, liquid–liquid extraction; IA, immunoassay; RIA, radioimmunoassay; CLIA, chemiluminesc
Analytical and preanalytical validation of a new mass spectrometric serum 5-hydroxyindoleacetic acid assay as neuroendocrine tumor marker
Keywords: LOQ، محدودیت مقدار; 5-HIAA, 5-hydroxyindoleacetic acid; NET, neuroendocrine tumor; LC-MS/MS, liquid chromatography tandem mass spectrometry; CgA, chromogranin A; LOQ, limit of quantitation; LOD, limit of detection; SPE, solid phase extractionLC-MS/MS; Neuroendocrine tumor; 5
Optimization of an HPLC method for phenylalanine and tyrosine quantization in dried blood spot
Keywords: LOQ، محدودیت مقدار; DBS, dried blood spot; HCl, hydrochloric acid; HPA, hyperphenylalaninemia; HPLC, high-performance liquid chromatography; LOD, limit of detection; LOQ, limit of quantitation; OPA-3-MPA, o-phthaldehyde-3-mercaptopropionic acid; PAH, phenylalanine hydroxylas
A novel HPLC-electrochemical detection approach for the determination of d-penicillamine in skin specimens
Keywords: LOQ، محدودیت مقدار; d-Pen, d-penicillamine; IS, internal standard; DTE, dithioerythritol; SPE, solid phase extraction; EPS, elastosis perforans serpiginosa; p-PXE, pseudo-pseudoxantoma elasticum; RSD, relative standard deviation; LOQ, limit of quantitation; LOD, limit of det
A gas chromatography–mass spectrometry assay to quantify camphor extracted from goat serum
Keywords: LOQ، محدودیت مقدار; BW, body weight; GC-FID, gas chromatograph-flame ionization detection; GC–MS, gas chromatography–mass spectrometry; IS, internal standard; LOD, limit of detection; LOQ, limit of quantitation; RSD, relative standard deviation; S.D., standard deviation; SIM
Determination of salivary testosterone and androstendione by liquid chromatography–tandem mass spectrometry
Keywords: LOQ، محدودیت مقدار; LC–MS/MS, liquid chromatography–tandem mass spectrometry; LOQ, limit of quantitation; ESI, electrospray ionizationSalivary testosterone; Salivary androstendione; Androgens; LC–MS/MS; ESI
Preanalytical factors and reference intervals for serum hepcidin LC–MS/MS method
Keywords: LOQ، محدودیت مقدار; LC, liquid chromatography; MS, mass spectrometry; ELISA, enzyme-linked immunosorbent assay; ISTD, internal standard; FDA, US Food and Drug Administration; LOD, limit of detection; LOQ, limit of quantitation; NRS, normal rabbit serum; SD, standard deviatio
Biomarkers of dementia: Comparison of electrochemiluminescence results and reference ranges with conventional ELISA
Keywords: LOQ، محدودیت مقدار; AD, Alzheimer’s disease; CSF, cerebrospinal fluid; CV, coefficient of variation; ECL, electrochemiluminescence; ELISA, enzyme-linked immunosorbant assay; LoB, limit of blank; LoD, limit of detection; LoQ, limit of quantitation; MCI, mild cognitive impairm
Fetal bisphenol A exposure: Concentration of conjugated and unconjugated bisphenol A in amniotic fluid in the second and third trimesters
Keywords: LOQ، محدودیت مقدار; BPA, bisphenol A; CV, coefficient of variation; HPLC, high-performance liquid chromatography; IS, internal standard; LOD, limit of detection; LOQ, limit of quantitation; LC–MS, liquid chromatography–mass spectrometry; QC, quality control; SPE, solid phase
Analytical method development for synthesized conjugated metabolites of trans-resveratrol, and application to pharmacokinetic studies
Keywords: LOQ، محدودیت مقدار; APAP, acetaminophen; CS, calibration standards; IA, intra-arterial administration; IS, internal standard; LC–MS/MS, liquid chromatography with tandem mass spectrometry; LOQ, limit of quantitation; MRM, multiple reaction monitoring; NaOMe, sodium methoxide
Analysis of inorganic chloramines in water
Keywords: LOQ، محدودیت مقدار; EI, Electron impact; GC, Gas chromatography; HPLC, High-performance liquid chromatography; LLE, Liquid-liquid extraction; LOQ, Limit of quantitation; MRM, Multiple-reaction monitoring; MS, Mass spectrometry; SPE, Solid-phase extractionAmperometry; Chemica
Biosynthesis and stereoselective analysis of (−)- and (+)-zaltoprofen glucuronide in rat hepatic microsomes and its application to the kinetic analysis
Keywords: LOQ، محدودیت مقدار; LOD, limit of detection; LOQ, limit of quantitation; RP-HPLC, reverse phase high performance liquid chromatography; UGT, uridine 5-diphosphoglucuronosyl transferases; UDPGA, uridine 5-diphosphoglucuronic acidZaltoprofen; Glucuronide; RP-HPLC; Kinetic anal
Urinary metanephrines by liquid chromatography tandem mass spectrometry: Using multiple quantification methods to minimize interferences in a high throughput method
Keywords: LOQ، محدودیت مقدار; ESI, electrospray ionization; GC–MS, gas chromatography mass spectrometry; LC–MS/MS, liquid chromatography tandem mass spectrometry; LOD, limit of detection; LOQ, limit of quantitation; MN, metanephrine; MRM, multiple reaction monitoring; NMN, normetaneph
Qualification of a microfluidics-based electrophoretic method for impurity testing of monoclonal antibodies
Keywords: LOQ، محدودیت مقدار; LOQ, limit of quantitation; QCs, quality control sample; mAb, monoclonal antibody; ANOVA, analysis of variances; TCA, time-corrected areaMicrofluidics-based; Electrophoresis; Qualification; Monoclonal antibody; Quality control
Analysis of in vitro release through reconstructed human epidermis and synthetic membranes of multi-vitamins from cosmetic formulations
Keywords: LOQ، محدودیت مقدار; RHE, reconstructed human epidermis; egf, epidermis growth factor; W/O, water in oil; O/W, oil in water; Ps, coefficient of permeability; LOD, limit of detection; LOQ, limit of quantitation; DTT, (dl)-Dithiothreitol; TFA, trifluoroacetic acidVitamins; RHE;
Method development and validation of capillary sodium dodecyl sulfate gel electrophoresis for the characterization of a monoclonal antibody
Keywords: LOQ، محدودیت مقدار; cSDS, capillary sodium dodecy sulfate gel electrophoresis; mAb1, monoclonal antibody; IAM, iodoacetamide; 2-ME, 2-mercaptoethanol; LOQ, limit of quantitation; SDS-PAGE, sodium dodecyl sulfate-polyacrylamide gel electrophoresis; HC, heavy chain; LC, light
Occurrence of patulin and its dietary intake through apple juice consumption by the Spanish population
Keywords: LOQ، محدودیت مقدار; PAT, patulin; MEKC, micellar electrokinetic chromatography method; PMTDI, provisional maximum tolerable daily intake; TDI, tolerable daily intake; DAD, diode array detection; LOD, limit of detection; LOQ, limit of quantitation; BW, body weightPatulin; Myc
Analytical performance characteristics of the Abbott Architect i2000 Tacrolimus assay; comparisons with liquid chromatography-tandem mass spectrometry (LC-MS/MS) and Abbott IMx methods
Keywords: LOQ، محدودیت مقدار; CI, confidence interval; LOQ, limit of quantitation; LC-MS/MS, liquid chromatography-tandem mass spectrometryTacrolimus; FK-506; Transplantation; Drug monitoring; Functional sensitivity; Method evaluation
Analysis of PFOA in dosed CD-1 mice. Part 2: Disposition of PFOA in tissues and fluids from pregnant and lactating mice and their pups
Keywords: LOQ، محدودیت مقدار; ANOVA, analysis of variance; BW, body weight; GD, gestational day; LOD, limit of detection; LOQ, limit of quantitation; MS, mass spectrometer; PFAA, perfluoroalkyl acid; PFOA, perfluorooctanoic acid; PFOS, perfluorooctane sulfonate; PND, postnatal day; SE
Phosphorus recovery from sewage sludge with a hybrid process of low pressure wet oxidation and nanofiltration
Keywords: LOQ، محدودیت مقدار; Phosphorus recovery; Nanofiltration; LOPROX; Wet oxidation; Sewage sludgebarg, relative pressure (bar gauge); LAS, linear alkylbenzene sulfonate; LOQ, limit of quantitation; LOPROX, low pressure wet oxidation; MAP, magnesium-ammonium-phosphate; NF, nanofi
A specific qualitative and real-time PCR detection of MON863 maize based on the 5′-transgene integration sequence
Keywords: LOQ، محدودیت مقدار; LM PCR; Qualitative PCR; TaqMan real-time PCR; MON863GM, genetically modified; GMOs, genetically modified organisms; LM PCR, ligation mediated PCR; LOD, limit of detection; LOQ, limit of quantitation; PCR, polymerase chain reaction; SD, standard deviation
Identification of volatile organic compounds secreted from cancer tissues and bacterial cultures
Keywords: LOQ، محدودیت مقدار; AR, acetone ratio; CT, computer tomography; DMS, dimethyl sulfide; DMDS, dimethyl disulfide; GC, gas chromatography; HS, head space; LOD, limit of detection; LOQ, limit of quantitation; MRI, magnetic resonance imaging; MS, mass spectrometry; PHA, phytohem
Assessment of dioxin and dioxin-like compounds in mainstream smoke from selected US cigarette brands and reference cigarettes
Keywords: LOQ، محدودیت مقدار; EMPC, estimated maximum possible concentration; FTC, federal trade commission; HAH, halogenated aromatic hydrocarbons; HY, high yield; ISO, International Organization for Standardization; LOD, limit of detection; LOQ, limit of quantitation; LY, low yield;
Measurement of voriconazole in serum and plasma
Keywords: LOQ، محدودیت مقدار; CYP, cytochrome P-450; Cmax, maximum plasma concentration; AUC, area under the curve; LOD, limit of detection; LOQ, limit of quantitation; SD, standard deviation; CV, coefficient of variation; RT, ambient (room) temperature; EDTA, potassium ethylenediamin
Measurement of CGRP in dried blood spots using a modified sandwich enzyme immunoassay
Keywords: LOQ، محدودیت مقدار; Ab, antibody; AchE, acetylcholine esterase; BSA, bovine serum albumin; CGRP, calcitonin gene-related peptide; EIA, enzyme immunoassay; ELISA, enzyme-linked immunosorbent assay; LOD, limit of detection; LOQ, limit of quantitation; PACAP, pituitary adenylat
Simultaneous determination of formic acid and formaldehyde in pharmaceutical excipients using headspace GC/MS
Keywords: LOQ، محدودیت مقدار; FID, flame ionization detector; GC/MS, gas chromatography/mass spectrometry; HPMC, high performance liquid chromatography; HPMC, hydroxypropyl methylcellulose; LOQ, limit of quantitation; PEG 3500, polyethylene glycol 3500; PEG 4000, polyethylene glycol 4
Capillary electrophoretic analysis of the antibiotic vancomycin in innovative microparticles and in commercial formulations
Keywords: LOQ، محدودیت مقدار; BGE, background electrolyte; EOF, electroosmotic flow; LOD, limit of detection; LOQ, limit of quantitation; SDS, sodium dodecyl sulphateVancomycin; Capillary zone electrophoresis; Glycopeptide antibiotic; Innovative microparticles; Controlled vancomycin r
Event-specific qualitative and quantitative PCR detection of MON863 maize based upon the 3′-transgene integration sequence
Keywords: LOQ، محدودیت مقدار; Qualitative and quantitative PCR; GMOs; Event-specific detection; MON863; TAIL-PCR; Transgene integrationGMOs, genetically modified organisms; GMPs, genetically modified plants; LOD, limit of detection; LOQ, limit of quantitation; PCR, polymerase chain re