کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
1241409 | 1495736 | 2007 | 6 صفحه PDF | دانلود رایگان |
Single-walled carbon nanotubes were produced by the conventional arc discharge method, and purified with a two-step treatment. First, the raw soot containing single-walled carbon nanotubes was burned up at ca. 350 °C in air to remove amorphous carbon, and then it was treated by strong acidic solvents to remove metal catalysts. Near-edge X-ray absorption fine structure spectroscopy was applied to analyze the defects on single-walled carbon nanotubes in whole purification process, so the experimental conditions can be optimized, and finally high-purity single-walled carbon nanotubes were obtained as revealed by various spectroscopic characterizations such as scanning electron microscopy, transmission electron microscopy, thermogravimetric analysis, and Raman spectroscopy.
Journal: Spectrochimica Acta Part B: Atomic Spectroscopy - Volume 62, Issues 6–7, July 2007, Pages 711–716