کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
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1308008 | 975161 | 2010 | 6 صفحه PDF | دانلود رایگان |
A new nano-sized lead(II) coordination polymer of maleic acid (H2Mal), [Pb(μ7-Mal)]n (1), has been synthesized by sonochemical method and characterized by scanning electron microscopy, X-ray powder diffraction, elemental analyses and IR spectroscopy. The compound 1 was structurally characterized by single-crystal X-ray diffraction. Thermal stability of nano and bulk samples of compound 1 were studied and compared with each other. After calcination of nano-sized compound 1 at 600 °C, pure phase micro-sized lead(II) oxide has been produced.
A new nano-sized lead(II) coordination polymer of maleic acid (H2Mal), [Pb(μ7-Mal)]n (1), has been synthesized by sonochemical method and characterized by scanning electron microscopy, X-ray powder diffraction, elemental analyses and IR spectroscopy. The compound 1 was structurally characterized by single-crystal X-ray diffraction. Thermal stability of nano and bulk samples of compound 1 were studied and compared with each other.Figure optionsDownload as PowerPoint slide
Journal: Inorganica Chimica Acta - Volume 363, Issue 11, 10 August 2010, Pages 2506–2511