کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
1652492 | 1517338 | 2007 | 5 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Effect of calcination conditions on phase formation and particle size of lead nickel niobate powders synthesized by using Ni4Nb2O9 precursor
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کلمات کلیدی
موضوعات مرتبط
مهندسی و علوم پایه
مهندسی مواد
فناوری نانو (نانو تکنولوژی)
پیش نمایش صفحه اول مقاله
چکیده انگلیسی
An approach to synthesize lead nickel niobate, Pb(Ni1/3Nb2/3)O3 or PNN, powders with a modified two-stage mixed oxide synthetic route has been developed. Novel intermediate phase of nickel diniobate (Ni4Nb2O9) was employed as a B-site precursor, with the formation of the PNN phase investigated as a function of calcination conditions by TG-DTA and XRD techniques. Morphology, particle size and chemical composition have been determined via a combination of SEM and EDX techniques. It has been found that the unreacted PbO and Pb1.45Nb2O6.26 phases tend to form together with PNN, depending on calcination conditions. It is seen that optimization of calcination conditions can lead to a 100% yield of PNN in a cubic phase.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Materials Letters - Volume 61, Issues 23â24, September 2007, Pages 4466-4470
Journal: Materials Letters - Volume 61, Issues 23â24, September 2007, Pages 4466-4470
نویسندگان
O. Khamman, R. Yimnirun, S. Ananta,