کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
5490272 | 1524788 | 2017 | 22 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Annealing temperature dependent structural and magnetic properties of MnFe2O4 nanoparticles grown by sol-gel auto-combustion method
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کلمات کلیدی
موضوعات مرتبط
مهندسی و علوم پایه
فیزیک و نجوم
فیزیک ماده چگال
پیش نمایش صفحه اول مقاله
چکیده انگلیسی
Manganese ferrite (MnFe2O4) nanoparticles were synthesized by sol-gel auto-combustion method using manganese nitrate and ferric nitrate as precursors and citric acid as a fuel. Scanning electron micrographs show irregularly shaped morphology of the particles. The as-prepared samples were annealed at 400, 500, 600 and 800 °C for 2 h in air. The phase identification and structural characterizations were performed using powder X-ray diffraction technique along with Mössbauer spectroscopy. Magnetization loops and 57Fe Mössbauer spectra were measured at RT. After annealing the sample at or below â¼ 500 °C, we observed two different spinel phases corresponding to two different lattice parameters. This is originating due to the partial oxidation of Mn2+ to Mn3+. At high annealing temperatures (â¼Â 600 °C or above) the spinel MnFe2O4 phase decomposes into crystalline α-Mn2O3 and α-Fe2O3 phases, and amorphous FeO phase.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Journal of Magnetism and Magnetic Materials - Volume 433, 1 July 2017, Pages 29-34
Journal: Journal of Magnetism and Magnetic Materials - Volume 433, 1 July 2017, Pages 29-34
نویسندگان
S.V. Bhandare, R. Kumar, Anupama A.V., H.K. Choudhary, V.M. Jali, B. Sahoo,