کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
1411411 | 1501860 | 2009 | 6 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Cyclic oxaalkyl diamide of o-phthalic acid as a new macrocyclic ligand for complexation of Li+ cation
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موضوعات مرتبط
مهندسی و علوم پایه
شیمی
شیمی آلی
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چکیده انگلیسی
Cyclic diamide of o-phthalic acid (CPhDA) was synthesised in the reaction between phtalic anhydride and 1,2-bis(2-aminoethoxy)ethane in high dilution conditions and its ability to form the 1:1 and 2:1 complexes with Li+ cations was detected by ESI mass spectrometry. The 1:1 complex was obtained in the solid state and studied by X-ray diffraction, FT-IR, NMR and PM5 semiempirical methods. The structure of 1:1 complex was also studied in acetonitrile. It was found that the structures of 1:1 complex are different in the solid and in solution.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Journal of Molecular Structure - Volume 930, Issues 1–3, 30 July 2009, Pages 26–31
Journal: Journal of Molecular Structure - Volume 930, Issues 1–3, 30 July 2009, Pages 26–31
نویسندگان
Adam Huczyński, Małgorzata Ratajczak-Sitarz, Andrzej Katrusiak, Bogumil Brzezinski,