کد مقاله کد نشریه سال انتشار مقاله انگلیسی نسخه تمام متن
1252971 971057 2008 5 صفحه PDF دانلود رایگان
عنوان انگلیسی مقاله ISI
Qualitative and Semi-quantitative Analysis of Quaternary Alkaloids in Coptis-scute Kerb Couple by Electrospray Mass Spectrometry
موضوعات مرتبط
مهندسی و علوم پایه شیمی شیمی (عمومی)
پیش نمایش صفحه اول مقاله
Qualitative and Semi-quantitative Analysis of Quaternary Alkaloids in Coptis-scute Kerb Couple by Electrospray Mass Spectrometry
چکیده انگلیسی
A practical solution of qualitatively analyzing quaternary alkaloids in coptis-scute herb couple by electrospray ionization mass spectrometry(ESl-MS) was developed. Without the complicated pretreatment of sample, the active ingredients including berberine, palmatine, coptisine, jatrorrhizine, epiberberine, and columbamine were identified and some relative content changing rules of alkaloids in coptis-scute couple were summarized in this article. The overall profiles of the complex extracts were obtained. After adding an internal standard(rutaecarpine), semi-quantitative analysis was performed and the result indicates that the actual content of alkaloids was decreased by increasing the amount of scute. Based on the data obtained by high-performance capillary electrophoresis(HPCE). the feasibility of semi-quantitative analysis by ES1-MS was further proved.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Chemical Research in Chinese Universities - Volume 24, Issue 2, March 2008, Pages 162-166
نویسندگان
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