کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
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1266985 | 972311 | 2011 | 4 صفحه PDF | دانلود رایگان |
A facile, efficient and environment-friendly protocol for the synthesis of 4-hydroxy-6-methyl-3-(1-(phenylimino)ethyl)-2H-pyran-2-one derivatives has been developed by the convenient ultrasound-mediated condensation of amine with dehydroacetic acid. This method provides several advantages over current reaction methodologies including a simple work-up procedure, shorter reaction times and higher yields.
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► A series of 4-hydroxy-6-methyl-3-(1-(phenylimino)ethyl)-2H-pyran-2-one derivatives have been synthesized under ultrasound irradiation.
► Ultrasonic irradiation was found to have beneficial effect on the synthesis of these Schiff bases.
► All the proposed reactions allowed the preparation of products in good yield without any further complicated refinement.
Journal: Ultrasonics Sonochemistry - Volume 18, Issue 5, September 2011, Pages 1048–1051