کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
1270170 | 972479 | 2012 | 6 صفحه PDF | دانلود رایگان |
![عکس صفحه اول مقاله: Sonocatalyzed facile and mild one pot synthesis of gem-dichloroaziridine derivatives under alkaline conditions Sonocatalyzed facile and mild one pot synthesis of gem-dichloroaziridine derivatives under alkaline conditions](/preview/png/1270170.png)
In this research, rapid and efficient preparation of 2,2-dichloro-1,3-diarylaziridines through the reaction of Schiff base compounds with dichlorocarbene yielded in situ from chloroform and sodium hydroxide without any phase transfer catalyst under ultrasonic irradiation is described. The advantages of this reaction are very short reaction times, excellent product yields, simplicity of the method and high purity of products.
In this research, rapid and efficient preparation of 2,2-dichloro-1,3-diarylaziridines through the reaction of Schiff base compounds with dichlorocarbene yielded in situ from chloroform and sodium hydroxide without any phase transfer catalyst under ultrasonic irradiation is described. The advantages of this reaction are very short reaction times, excellent product yields, simplicity of the method and high purity of products.Figure optionsDownload as PowerPoint slideHighlights
► Ultrasonic irradiation catalyzed synthesis of gem-dichloroaziridines.
► Any PTC was needed for this reaction under ultrasonic conditions.
► Products were obtained in excellent yields and short reaction times.
► Simplicity of the method and high purity of products.
Journal: Ultrasonics Sonochemistry - Volume 19, Issue 1, January 2012, Pages 130–135