کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
1799033 | 1524833 | 2015 | 5 صفحه PDF | دانلود رایگان |
• CoFe2O4 nanospheres were prepared by hydrothermal synthesis for the first time.
• Average grain size was found to be 180 nm.
• Its structural, morphological, magnetic behavior was studied.
• TEM observations confirmed the spherical morphology of the mesoporous ferrites.
Mesoporous CoFe2O4 nanospheres with an average size of 180 nm were fabricated via a facile hydrothermal process using ethylene glycol as solvent and sodium acetate (NaAc) as electrostatic stabilizer. In this method, ethylene glycol plays a vital role in the formation of cobalt nanoospheres as a solvent and reducing agent. The structure and morphology of the prepared materials were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), high-resolution TEM (HRTEM), Fourier transform infrared spectroscopy (FTIR) and X-ray photoelectron spectroscopy (XPS). The nanospheres exhibited ferromagnetic properties with high saturation magnetization value of about 60.19 emu/g at room temperature. The BET surface area of the nanospheres was determined using the nitrogen absorption method. The porous CoFe2O4 nanospheres displayed good magnetic properties, which may provide a very promising candidate for their applications in target drug delivery.
Journal: Journal of Magnetism and Magnetic Materials - Volume 388, 15 August 2015, Pages 40–44