کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
228084 | 464834 | 2013 | 7 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Optimization of process parameters using D-optimal design for synthesis of ZnO nanoparticles via sol–gel technique
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کلمات کلیدی
موضوعات مرتبط
مهندسی و علوم پایه
مهندسی شیمی
مهندسی شیمی (عمومی)
پیش نمایش صفحه اول مقاله
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چکیده انگلیسی
The experimental conditions for the synthesis of ZnO nanoparticles to produce minimal size were optimized using the D-optimal design. The influence of process parameters involves molar ratio of the starting materials, pH and the calcination temperature on the particle size were evaluated using the polynomial regression. The optimum conditions revealed by the model for obtaining a minimum particle size of ZnO were predicted to have a molar ratio of 1.76, pH of 1.50 and calcination at 402.2 °C. The obtainable particle size upon applying the model is 22.9 nm in compare to experimental result of 18 ± 2 nm was obtained.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Journal of Industrial and Engineering Chemistry - Volume 19, Issue 1, 25 January 2013, Pages 99–105
Journal: Journal of Industrial and Engineering Chemistry - Volume 19, Issue 1, 25 January 2013, Pages 99–105
نویسندگان
Muneer M. Ba-Abbad, Abdul Amir H. Kadhum, Abu Bakar Mohamad, Mohd S. Takriff, Kamaruzzaman Sopian,