Wear performances of surface hardened PM steel from pre-alloyed powder

Powder metallurgy (PM) processing of steels typically results in a material characterized by residual porosity reducing the mechanical strength of the material. That is why mechanical components produced from PM steels for high demanding applications often require a surface hardening in order to improve both the fatigue and the wear resistance. Among the surface treatments, gas nitriding assures economic advantages but the presence of interconnected porosity also makes the core structure involved by the diffusional phenomena. In this paper gas nitriding is proposed in combination with shot peening, as a surface densification technique, to improve the wear performances of PM components from prealloyed powder. 40 mm diameter, 9.85 mm thickness disks were pressed at 7.0 g/cm3 density from a pre-alloyed powder (1.5% Cr, 0.5% Mo), with 0.8% graphite. The disks were sintered at 1120 °C, 30 min, in N2–H2 (90–10) atmosphere in an industrial equipment. Four conditions of the disks were examined: as-sintered, sintered and gas nitrided, sintered and shot-peened, sintered-shot peened-gas nitrided. The disks were characterized by experimental tests: dimensional variations, macro and microhardness profiles, LOM observations, surface texture analysis, residual stress analysis by X-Ray technique and pin on disk wear tests. The results of the wear tests were fulfilled with observations by SEM and new interesting interpretations of the involved mechanisms were proposed by the application of the energetic approach and non-standard wear tests.

► Gas nitriding and a pre-nitriding densification by shot-peening on a Cr based sintered steel are carried out.
► The effects on the microstructural characteristics and the wear resistance have been studied.
► Non standard wear tests have been performed.
► Energetic approaches have been introduced in the discussion of the results.