کد مقاله کد نشریه سال انتشار مقاله انگلیسی نسخه تمام متن
745097 894413 2009 5 صفحه PDF دانلود رایگان
عنوان انگلیسی مقاله ISI
Amperometric glucose sensor based on 3D ordered nickel–palladium nanomaterial supported by silicon MCP array
موضوعات مرتبط
مهندسی و علوم پایه شیمی شیمی آنالیزی یا شیمی تجزیه
پیش نمایش صفحه اول مقاله
Amperometric glucose sensor based on 3D ordered nickel–palladium nanomaterial supported by silicon MCP array
چکیده انگلیسی

A novel silicon-based amperometric sensor for the determination of glucose is described. In this sensor, Ni–Pd nanoparticles as the sensing materials adhere onto a supporter comprising the 3D ordered silicon microchannel plate (MCP) serving as the electrode. The 3D ordered Si MCP is fabricated by electrochemical etching, and the Ni–Pd nanoparticles are obtained by electroless deposition of nickel and palladium onto the sidewall of the MCP followed by annealing at 300 °C under argon to stabilize the structure. Scanning electron microscopy (SEM), energy-dispersive X-ray spectrometry (EDS), and electrochemical methods are adopted to characterize the Ni–Pd/Si-MCP nanocomposite sensing electrode. This nanocomposite material shows good electrocatalytic activity towards the oxidation of glucose in alkaline solutions. They exhibit very strong and sensitive current responses to glucose even in the presence of high concentrations of interfering species, in addition to showing excellent long-term stability and good reproducibility.

ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Sensors and Actuators B: Chemical - Volume 141, Issue 1, 18 August 2009, Pages 338–342
نویسندگان
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