کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
7642253 | 1494870 | 2016 | 4 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Sensitive voltammetric determination of melittin in honeybee venom powder from Apis mellifera
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کلمات کلیدی
موضوعات مرتبط
مهندسی و علوم پایه
شیمی
شیمی آنالیزی یا شیمی تجزیه
پیش نمایش صفحه اول مقاله
![عکس صفحه اول مقاله: Sensitive voltammetric determination of melittin in honeybee venom powder from Apis mellifera Sensitive voltammetric determination of melittin in honeybee venom powder from Apis mellifera](/preview/png/7642253.png)
چکیده انگلیسی
In this study a gold electrode was used to indirect determination of melittin in nonaqueous medium by square wave stripping voltammetric (SWSV) method. The method is based on measuring the decrease of oxidation peak current of ferrocene with addition melittin. The optimum conditions include an accumulation potential of 0Â mV (versus Ag/Ag+), an accumulation time of 10Â s. A calibration curve was obtained for melittin in a linear range of 40 to 240Â nM with a low detection limit (LOD) of 12Â nM (at a signal-to-noise ratio of 3). The validated SWSV method showed good linearity as well as satisfactory repeatability and immediate precision values, for both instrument and method. The method was successfully applied to the determination of melittin in honeybee venom sample.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Microchemical Journal - Volume 124, January 2016, Pages 364-367
Journal: Microchemical Journal - Volume 124, January 2016, Pages 364-367
نویسندگان
Ummihan Taskoparan Yilmaz, Tugba Melekogullari, Aysel Kekillioglu, Demet Uzun,