کد مقاله کد نشریه سال انتشار مقاله انگلیسی نسخه تمام متن
776219 1463482 2014 7 صفحه PDF دانلود رایگان
عنوان انگلیسی مقاله ISI
Preparation and performance of ceramizable heat-resistant organic adhesive for joining Al2O3 ceramics
موضوعات مرتبط
مهندسی و علوم پایه سایر رشته های مهندسی مهندسی مکانیک
پیش نمایش صفحه اول مقاله
Preparation and performance of ceramizable heat-resistant organic adhesive for joining Al2O3 ceramics
چکیده انگلیسی

Ceramizable heat-resistant organic adhesive (CHA) was prepared by using preceramic polymer polysiloxane as matrix, TiB2 ceramic powder and low melting point glass powder as additives. The curing mechanism, thermal stability properties, phase composition after pyrolysis, structural evolution of bonding layer and bonding mechanism of the adhesive were investigated by FTIR, TGA-DSC, XRD, SEM, FESEM and bonding strength tests. Results of bonding tests showed the maximum shear strength of the joints was 21 MPa when heat treatment at 1200 °C for 2 h in air. Polysiloxane resin acted as crosslinking adhesive at low temperatures and tended to convert to ceramic bonding layer at high temperatures, resulting from ceramization reaction with active fillers. The formation and growth of ceramic phase after heat treatment enhanced the thermal stability and bonding performance of the adhesive at high temperature.

ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: International Journal of Adhesion and Adhesives - Volume 55, December 2014, Pages 132–138
نویسندگان
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