Fracture toughness of a directionally solidified Al–Nb–Ni ternary eutectic

Fracture toughness (KIC), an important property of brittle materials, can be determined by indentation cracking tests. This paper reports on an investigation of the fracture toughness of a directionally solidified Al3Nb–Nb2Al–AlNbNi ternary eutectic, based on the Vickers indentation test applied to longitudinal and transverse sections of its microstructure. The measurements were taken using indentation loads varying from 2.45 to 24.5 N. Correlations between the resulting crack parameters and indentation load were evaluated using Palmqvist and half-penny cracks models. In the range of indentation loads studied, the results suggested that the Palmqvist model provided a better fit to the experimental data. Fracture toughness was calculated using equations developed for Palmqvist crack mode. The indentation fracture toughness values for longitudinal and transverse sections are in the range of 2.82–3.05 MPa m1/2 and 2.98–3.59 MPa m1/2, respectively. It was found that the addition of Ni and incorporation of a third phase to the Al3Nb–Nb2Al eutectic improved fracture toughness of this in situ composite material.

► Fracture toughness of a ternary eutectic in the Al–Nb–Ni system was investigated using Vickers indentations.
► Fracture toughness for longitudinal and transverse sections are in the range of 2.82–3.05 MPa m1/2 and 2.98–3.59 MPa m1/2.
► Poisson’s ratio and Young’s modulus of the Al–Nb–Ni ternary eutectic were found to be, respectively, 0.269 and 251 GPa.
► Addition of AlNbNi phase to Al3Nb–Nb2Al eutectic that results in Al3Nb–Nb2Al–AlNbNi eutectic, increased fracture toughness.