
Purification of five azaspiracids from mussel samples contaminated with DSP toxins and azaspiracids
Keywords: SPE، استخراج فاز جامد; AZA, azaspiracid; DSP, diarrhoetic shellfish poisoning; SPE, solid phase extraction; HPLC, high-performance liquid chromatography; LC/MS, liquid chromatography coupled to mass spectrometry; YTX, yessotoxin; DTX, dinophysistoxin; OA, okadaic acid; HP, hepa