کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
10556840 | 968435 | 2011 | 8 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
A clean up step of fat content previous to trace metal characterization in mussel tissues by inductively coupled plasma mass spectrometry
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کلمات کلیدی
موضوعات مرتبط
مهندسی و علوم پایه
شیمی
شیمی آنالیزی یا شیمی تجزیه
پیش نمایش صفحه اول مقاله
![عکس صفحه اول مقاله: A clean up step of fat content previous to trace metal characterization in mussel tissues by inductively coupled plasma mass spectrometry A clean up step of fat content previous to trace metal characterization in mussel tissues by inductively coupled plasma mass spectrometry](/preview/png/10556840.png)
چکیده انگلیسی
Inductively coupled plasma mass spectrometry analysis of trace and major elements of mussel tissues can be quickly and accurately analyzed after cleaning up the interfering fat content before the sample is digested in a microwave oven. Making use of experimental designs, the clean up procedure was achieved by the extraction of 1Â g of freeze-dried tissue sample stirred with 5Â ml of dichloromethane during five minutes. The microwave assisted digestion of the fat free samples was carried out with 0.2Â g of tissue sample, 15Â ml of 7.0% nitric acid with a power of 980Â W during 18Â min. The analytical method efficiency (accuracy and precision) was evaluated with a CRM: (NIST 2977, mussel tissue) and real mussel samples analyzed previously. The results confirmed the accuracy of the analysis by agreement with the previous results but the precision was significantly improved. The developed method allows operating routinely permitting to large numbers of samples to be quickly screened for trace metals.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Microchemical Journal - Volume 99, Issue 2, November 2011, Pages 252-259
Journal: Microchemical Journal - Volume 99, Issue 2, November 2011, Pages 252-259
نویسندگان
J.C. Raposo, U. Villanueva, L. Bartolomé, M. Olivares, J.A. Carrero, A. Sarmiento, N. Etxebarria, J.M. Madariaga,