کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
10638100 | 995352 | 2011 | 5 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Sol-gel preparation and characterization of non-substituted and Sr-substituted gadolinium cobaltates
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موضوعات مرتبط
مهندسی و علوم پایه
مهندسی مواد
مواد الکترونیکی، نوری و مغناطیسی
پیش نمایش صفحه اول مقاله
چکیده انگلیسی
An aqueous sol-gel chemistry approach for the preparation of Sr-substituted perovskite gadolinium cobaltates Gd1âxSrxCoO3âδ (x = 0.0, 0.25, 0.5 and 0.75) has been applied. The metal ions, generated by dissolving starting materials in diluted acetic acid were complexed by EDTA to obtain the precursors for non-substituted and Sr-substituted GdCoO3. However, only two single-phase cobaltate samples with x = 0.0 and 0.25 have been obtained by the suggested sol-gel method. The influences of synthesis temperature and the amount of substituent on the phase purity of Gd1âxSrxCoO3âδ were investigated. The evolution of the gels during heating, composition and micro-structural features in the polycrystalline samples was studied by thermal analysis (TG/DSC), infrared spectroscopy (IR), powder X-ray diffraction analysis (XRD) and scanning electron microscopy (SEM).
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Materials Chemistry and Physics - Volume 125, Issue 3, 15 February 2011, Pages 469-473
Journal: Materials Chemistry and Physics - Volume 125, Issue 3, 15 February 2011, Pages 469-473
نویسندگان
S. Cizauskaite, S. Johnsen, J.-E. Jørgensen, A. Kareiva,