Ultrasonic dyeing of cellulose nanofibers

• We report ultrasonic dyeing of nanofibers for the very first time.
• Cellulose nanofibers were dyed with anionic reactive dyes.
• Ultrasonic dyeing by batchwise method for nanofibers was optimized.
• Ultrasonic dyeing resulted higher color yield than the conventional dyeing.
• Color fastness test results depicted good dye fixation.

Textile dyeing assisted by ultrasonic energy has attained a greater interest in recent years. We report ultrasonic dyeing of nanofibers for the very first time. We chose cellulose nanofibers and dyed with two reactive dyes, CI reactive black 5 and CI reactive red 195. The cellulose nanofibers were prepared by electrospinning of cellulose acetate (CA) followed by deacetylation. The FTIR results confirmed complete conversion of CA into cellulose nanofibers. Dyeing parameters optimized were dyeing temperature, dyeing time and dye concentrations for each class of the dye used. Results revealed that the ultrasonic dyeing produced higher color yield (K/S values) than the conventional dyeing. The color fastness test results depicted good dye fixation. SEM analysis evidenced that ultrasonic energy during dyeing do not affect surface morphology of nanofibers. The results conclude successful dyeing of cellulose nanofibers using ultrasonic energy with better color yield and color fastness results than conventional dyeing.

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