کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
1266418 | 972275 | 2011 | 5 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Sonochemical syntheses and characterization of nano-structured three-dimensional lead(II) coordination polymer constructed of fumaric acid
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کلمات کلیدی
موضوعات مرتبط
مهندسی و علوم پایه
شیمی
شیمی (عمومی)
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چکیده انگلیسی
Nano-structured three-dimensional lead(II) coordination polymer, [Pb(μ6-Fum)]n (1); {Fum = Fumarate}, has been synthesized by sonochemical method and characterized by scanning electron microscopy, X-ray powder diffraction, elemental analyses and IR spectroscopy. Solvent effects on size and morphology of nano-structured compound 1 have been studied. Calcination of the nano-sized compound 1 at 600 °C under air atmosphere yields PbO nanoparticles. The thermal stability of compound 1 both its bulk and nano-size has been studied by thermal gravimetric (TG) and differential thermal (DTA) analyses and compared each other.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Ultrasonics Sonochemistry - Volume 18, Issue 1, January 2011, Pages 407–411
Journal: Ultrasonics Sonochemistry - Volume 18, Issue 1, January 2011, Pages 407–411
نویسندگان
Leila Aboutorabi, Ali Morsali,