کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
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1336724 | 979608 | 2010 | 4 صفحه PDF | دانلود رایگان |
![عکس صفحه اول مقاله: Synthesis and characterization of new air stable primary amido substituted diborane(4) derivatives Synthesis and characterization of new air stable primary amido substituted diborane(4) derivatives](/preview/png/1336724.png)
Three new diborane(4) derivatives, 1,2-bis(2,4,6-trimethylanilide)-1,2-bis(dimethyamido)diborane(4) (1), 1,2-bis(2,4,6-trimethylanilide)-1,2-bis(duryl)diborane(4) (2) and 1,2-bis(anilide)-1,2-bis(duryl)diborane(4) (3), have been synthesized and characterized by means of elemental analysis, IR, 1H, 13C and 11B NMR spectroscopy. Additionally, the structures of compounds 1 and 2 have been determined by the single crystal X-ray diffraction technique. The compounds 1 and 2 crystallize in the monoclinic P21/c space group. All of the compounds were found to be air stable.
New air stable primary amido substituted diborane(4) derivatives were prepared and characterized by elemental analysis, IR, 1H, 13C and 11B NMR spectroscopy. The structures of two compounds were determined by X-ray diffraction.Figure optionsDownload as PowerPoint slide
Journal: Polyhedron - Volume 29, Issue 5, 30 March 2010, Pages 1465–1468