کد مقاله کد نشریه سال انتشار مقاله انگلیسی نسخه تمام متن
144490 438935 2011 5 صفحه PDF دانلود رایگان
عنوان انگلیسی مقاله ISI
Microwave-assisted hydrothermal synthesis of ZnO rod-assembled microspheres and their photocatalytic performances
موضوعات مرتبط
مهندسی و علوم پایه مهندسی شیمی مهندسی شیمی (عمومی)
پیش نمایش صفحه اول مقاله
Microwave-assisted hydrothermal synthesis of ZnO rod-assembled microspheres and their photocatalytic performances
چکیده انگلیسی

ZnO rod-assembled microspheres were successfully fabricated by using the microwave-assisted hydrothermal method in the existence of the poly ethylene glycol (PEG) with the molecular weight of 2000. The structure and morphology of as-prepared samples were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) equipped with energy dispersive spectrometer (EDS), transmission electron microscopy (TEM) and selected area electron diffraction (SAED). The experimental results exhibit that the as-prepared ZnO microspheres with a diameter about 1.5–2.0 μm were composed of many rods with the diameter of 300 nm and the length of 1 μm, respectively. Photoluminescene measurement shows a broad visible emission band centered at around 500–560 nm. The improved catalytic activity may be attributed to structural difference, including morphology, surface orientation and surface defects. Furthermore, the possible growth and photodegradation mechanism of the as-prepared sample is also briefly discussed.

ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Advanced Powder Technology - Volume 22, Issue 4, July 2011, Pages 493–497
نویسندگان
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