کد مقاله کد نشریه سال انتشار مقاله انگلیسی نسخه تمام متن
1497790 1510825 2014 21 صفحه PDF دانلود رایگان
عنوان انگلیسی مقاله ISI
Recent progress in scanning electron microscopy for the characterization of fine structural details of nano materials
ترجمه فارسی عنوان
پیشرفت اخیر در میکروسکوپ الکترونی اسکن برای توصیف جزئیات ساختاری نانو مواد
موضوعات مرتبط
مهندسی و علوم پایه مهندسی مواد سرامیک و کامپوزیت
چکیده انگلیسی

Research concerning nano-materials (metal-organic frameworks (MOFs), zeolites, mesoporous silicas, etc.) and the nano-scale, including potential barriers for the particulates to diffusion to/from is of increasing importance to the understanding of the catalytic utility of porous materials when combined with any potential super structures (such as hierarchically porous materials). However, it is difficult to characterize the structure of for example MOFs via X-ray powder diffraction because of the serious overlapping of reflections caused by their large unit cells, and it is also difficult to directly observe the opening of surface pores using ordinary methods. Electron-microscopic methods including high-resolution scanning electron microscopy (HRSEM) have therefore become imperative for the above challenges. Here, we present the theory and practical application of recent advances such as through-the-lens detection systems, which permit a reduced landing energy and the selection of high-resolution, topographically specific emitted electrons, even from electrically insulating nano-materials.

ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Progress in Solid State Chemistry - Volume 42, Issues 1–2, May 2014, Pages 1–21
نویسندگان
, , , , , , , , , , , , , , , ,