کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
1517445 | 1511587 | 2010 | 7 صفحه PDF | دانلود رایگان |
![عکس صفحه اول مقاله: Hydrothermal synthesis of well-dispersed ultrafine N-doped TiO2 nanoparticles with enhanced photocatalytic activity under visible light Hydrothermal synthesis of well-dispersed ultrafine N-doped TiO2 nanoparticles with enhanced photocatalytic activity under visible light](/preview/png/1517445.png)
Ultrafine nitrogen-doped TiO2 nanoparticles with narrow particle size distribution, good dispersion, and high surface area were synthesized in the presence of urea and PEG-4000 via a hydrothermal procedure. TEM observation, N2 adsorption, XRD, UV–vis spectroscopy, the Raman spectroscopy and XPS analysis were conducted to characterize the synthesized TiO2 particles. The synthesized TiO2 particles were a mixture of 49.5% anatase and 50.5% rutile with a size of around 5 nm. The photocatalytic activities were tested in the degradation of an aqueous solution of a reactive Brilliant Blue KN-R under both UV and visible light. The synthesized TiO2 particles showed much higher photocatalytic activity than a commercial P25 TiO2 powder under both UV and visible light irradiations. The high performance is associated to N doping, the reduced particle size, good dispersion, high surface area, and a quantum size effect.
Journal: Journal of Physics and Chemistry of Solids - Volume 71, Issue 3, March 2010, Pages 156–162