کد مقاله کد نشریه سال انتشار مقاله انگلیسی نسخه تمام متن
1556375 999186 2013 6 صفحه PDF دانلود رایگان
عنوان انگلیسی مقاله ISI
One-step Synthesis of Shape-controllable Gold Nanoparticles and Their Application in Surface-enhanced Raman Scattering
موضوعات مرتبط
مهندسی و علوم پایه مهندسی مواد شیمی مواد
پیش نمایش صفحه اول مقاله
One-step Synthesis of Shape-controllable Gold Nanoparticles and Their Application in Surface-enhanced Raman Scattering
چکیده انگلیسی

Gold nanoparticles (NPs) of various shapes were synthesized by a one-step method at ambient temperature in the presence of NaCl. 2-mercaptosuccinic acid (MSA) was used as both reducing agent and stabilizing agent. The shapes of gold NPs were controllable by simply tuning S/Au ratio (S is from MSA molecule, and S/Au ratio is controlled by tuning the volume of added MSA solution), and triangle, polygonal and spherical nanoparticles were obtained. This result suggested a new way to consider the effects of MSA on the growth of nanoparticles, which showed that MSA is a strong capping agent and facilitates more uniform growth of nanoparticles in every dimension. And other important factors on nanoparticles growth including NaCl and temperature were discussed. Furthermore, a typical probe molecule, 4-aminothiophenol (4-ATP) was used to test the surface-enhanced Raman scattering (SERS) activity of these gold NPs and the results indicated good Raman activity on these substrates. And the enhancement factor (EF) at 1078 cm−1 (a1) was estimated to be as large as 6.3 × 104 and 5.5 × 104 for triangular plates and truncated particles, respectively.

ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Journal of Materials Science & Technology - Volume 29, Issue 7, July 2013, Pages 613–618
نویسندگان
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