Effect of pre-annealing treatment on the compressive deformation and damage behavior of ultrafine-grained copper

The effect of short-term pre-annealing treatment on the compressive deformation and damage behavior of ultrafine-grained (UFG) copper produced by equal channel angular pressing (ECAP) has been studied by mechanical tests and microstructural observations. It is found that a controlled 10-min pre-annealing treatment on the UFG copper below the recrystallization temperature can result obviously in a higher strength (higher flow stress level) and a higher flow stability (lower stress softening rate) under uniaxial compression, as compared to the case of as-ECAPed sample. Observations of surface and interior deformation damage features indicate that, compared to the as-ECAPed copper sample, the pre-annealed ECAPed copper at less than recrystallization temperature may exhibit a better compressive plastic deformation capacity, namely, the destructive deformation morphology of large-scale shear bands normally observed in compressed as-produced UFG copper sample would not appear in compressed pre-annealed sample, except for a relatively smooth surface morphology featuring some ‘step’ reliefs with a few discontinuous shear bands and non-propagation voids. Finally, the deformation mechanism of different kinds of severe plastic deformation (SPD) processed UFG materials as well as their pre-annealing effects are further discussed, and a general rule is summarized as follows: an appropriate selection of pre-annealing temperature and annealing time is needed for improving both strength and ductility of SPDed materials with a microstructure comprising equiaxed grains and well-defined grain boundaries.

► Appropriate pre-annealing treatment can improve compressive properties of UFG Cu.
► The pre-annealed UFG copper exhibits a better plastic deformation capacity.
► Pre-annealing effect on deformation mechanism of SPDed materials is discussed.