کد مقاله کد نشریه سال انتشار مقاله انگلیسی نسخه تمام متن
238677 465768 2009 9 صفحه PDF دانلود رایگان
عنوان انگلیسی مقاله ISI
Identification of models for control of wet granulation
موضوعات مرتبط
مهندسی و علوم پایه مهندسی شیمی مهندسی شیمی (عمومی)
پیش نمایش صفحه اول مقاله
Identification of models for control of wet granulation
چکیده انگلیسی

The modeling work in this paper provides insight on improved control and design (including measurement selection) of a granulation process. Two different control strategies (MPC and PID) are evaluated on an experimentally validated granulation model. This model is based on earlier work done at The University of Sheffield, UK and Organon, The Netherlands [C.F.W. Sanders, W. Oostra, A.D. Salman, M.J. Hounslow, Development of a predictive high-shear granulation model; experimental and modeling results, 7th World Congress of Chemical Engineering, Glasgow (2005), C11-002]. The granulation kinetics were measured in a 10 liter batch granulator with an experimental design that included four process variables. The aggregation rates were extracted with a Discretized Population Balance (DPB) model. Knowledge of the process kinetics was used to model a continuous (well mixed) granulator. The controller model for the Model Predictive Controller is a linearized state space model, derived from the nonlinear DPB model. It has the four process variables from the experimental design and a feed ratio as input variables. Since the DPB model describes the whole Granule Size Distribution (GSD), candidate sets of lumped output variables were evaluated. When measuring controller performance based on the full granule size distribution, it is shown that a PID controller can actually produce results that fluctuate more than the open-loop response. An MPC controller improves stability on both process outputs and the full granule size distribution. The work shows that measuring and controlling specific number based lumped outputs result in a more stable process than when mass based lumped outputs are used. The paper describes a general strategy of using lab scale batch experiments to design and control (small or large scale) continuous granulators. The continuous experiments in this paper are based on simulation, therefore future experimental validation will elucidate further the link between batch and continuous granulation.

A method for identification of linear state-space models is presented, for use in the development of a model predictive controller for a continuous granulator. The resulting controller is benchmarked against a traditional PID controller, using a 1-dimensional population balance model.Figure optionsDownload as PowerPoint slide

ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Powder Technology - Volume 188, Issue 3, 10 January 2009, Pages 255–263
نویسندگان
, , ,