کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
5350661 | 1503632 | 2015 | 8 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Synthesis and surface characterization of a patterned cuprite sample: Preparatory step in the evaluation scheme of an X-ray-excited optical microscopy system
ترجمه فارسی عنوان
سنتز و مشخصه سطح یک نمونه کریستالی الگو: مرحله آماده سازی در طرح ارزیابی یک سیستم میکروسکوپ نوری با سیستم اشعه ایکس
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کلمات کلیدی
موضوعات مرتبط
مهندسی و علوم پایه
شیمی
شیمی تئوریک و عملی
چکیده انگلیسی
The synthesis and characterization of a reference sample containing a distinct geometrical pattern of Cu2O (cuprite) are described. The sample is to be used as an assessment sample to evaluate a newly developed X-ray-excited optical luminescence (XEOL) microscope, built for non-destructive chemical imaging of metal and other surfaces. The sample was produced by heating in a reducing flame and subsequent air exposure. It was characterized both qualitatively and quantitatively using X-ray photoelectron spectroscopy (XPS), X-ray absorption spectroscopy in both fluorescence mode (XAS) and optical luminescence mode (XEOL-XAS) and X-ray diffraction (XRD). Results indicate the presence of a layered structure comprising a heterogeneous mixture of cuprite and tenorite (CuO) with mainly cuprite (91.4%) in the near-surface regions and larger amounts of tenorite in the top 1-3Â nm. The cuprite produced via this protocol was found to provide intense optical luminescence upon X-ray bombardment, which is particularly useful during the evaluation of the microscope.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Applied Surface Science - Volume 332, 30 March 2015, Pages 657-664
Journal: Applied Surface Science - Volume 332, 30 March 2015, Pages 657-664
نویسندگان
Pieter-Jan Sabbe, Mark G. Dowsett, Michel De Keersmaecker, Matthew Hand, Paul Thompson, Annemie Adriaens,