کد مقاله کد نشریه سال انتشار مقاله انگلیسی نسخه تمام متن
5352325 1388149 2013 9 صفحه PDF دانلود رایگان
عنوان انگلیسی مقاله ISI
Application of ultrasound irradiation on sol-gel technique for corrosion protection of Al65Cu20Fe15 alloy powder
موضوعات مرتبط
مهندسی و علوم پایه شیمی شیمی تئوریک و عملی
پیش نمایش صفحه اول مقاله
Application of ultrasound irradiation on sol-gel technique for corrosion protection of Al65Cu20Fe15 alloy powder
چکیده انگلیسی
Al65Cu20Fe15 alloy powder was firstly encapsulated by the conventional sol-gel technique utilizing tetraethoxysilane (TEOS) as the precursor in order to improve its corrosion resistance. The optimization was based on nine well-planned orthogonal experiments (L9 (34)). Four main factors in the encapsulation process (i.e. reaction temperature, ethylenediamine concentration, TEOS concentration and feeding method) were investigated. According to the visual analyses of the result, the optimum condition was obtained. Based on the optimal condition in the conventional sol-gel technique, the encapsulation process was then conducted under ultrasonic irradiation. The effects of ultrasound amplitude and irradiation time on the encapsulation process were also studied. FTIR, XRD, SEM, DLS and EDS were also used to characterize the resulting sample. Finally, the corrosion inhibition efficiency of encapsulated powder attained 99.3% in the acidic condition of pH 1, and the average grain size (d50) of the encapsulated powder was just 4.8% larger than that of the raw powder, implying that there was a thin silica film on the surface of powder.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Applied Surface Science - Volume 285, Part B, 15 November 2013, Pages 249-257
نویسندگان
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