کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
5356224 | 1388202 | 2015 | 9 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
The microstructure of polyamide 6 and polyamide 6/polyhedral oligomeric silsesquioxane nanocomposites synthesized by phase inversion procedure under electric field
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موضوعات مرتبط
مهندسی و علوم پایه
شیمی
شیمی تئوریک و عملی
پیش نمایش صفحه اول مقاله
چکیده انگلیسی
Polyamide 6 (PA6) and PA6/octaammonium POSS (OA-POSS) nanocomposites were synthesized by phase inversion procedure assisted with external electric field and characterized by X-ray diffraction (XRD), differential scanning calorimetry (DSC), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and water contact angle (CA) measurements. It is very interesting to find that external electric field has greatly different effects on the microstructure evolution behaviors of PA6 and PA6/OA-POSS nanocomposites. For pure PA6 samples, crystallization was retarded while hydrophilicity was enhanced with increasing the strength of applied electric field. However, for PA6/OA-POSS nanocomposites, both crystallinity and hydrophilicity keep stable with increased electric field strength. The migration behavior of OA-POSS molecules was hindered under electric field. The mechanism for the formation of PA6 and PA6/OA-POSS nanocomposites with the presence of external electric field is discussed.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Applied Surface Science - Volume 357, Part B, 1 December 2015, Pages 1454-1462
Journal: Applied Surface Science - Volume 357, Part B, 1 December 2015, Pages 1454-1462
نویسندگان
Qi Zhou, Yang Cong, Ningkun Wu, Leslie S. Loo,