کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
5357606 | 1503637 | 2015 | 43 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Elaboration and characterization of a multifunctional silane/ZnO hybrid nanocomposite coating
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کلمات کلیدی
موضوعات مرتبط
مهندسی و علوم پایه
شیمی
شیمی تئوریک و عملی
پیش نمایش صفحه اول مقاله

چکیده انگلیسی
The present study aims at investigating the elaboration of a ZnO/sol-gel nanocomposite coating, which can provide a number of properties such as UV-absorption, mechanical and barrier effects, etc. depending on targeted applications. The sol-gel coating formulation is an inorganic-organic hybrid based on tetraethoxysilane (TEOS) and glycidyloxypropyltrimethoxysilane (GPTMS). In order to ensure good dispersion in the sol-gel matrix, ZnO nanoparticles were surface-modified with a silane coupling agent. The functionalization was confirmed by Fourier transform infrared (FTIR) and thermogravimetric (TGA) analyses. Field emission gun-scanning electron microscopy (FEG-SEM) characterization of the nanocomposite film reveals a homogeneous distribution and dispersion of the ZnO nanoparticles throughout the film. Glow discharge optical emission spectrometry (GDOES) analysis allows evaluating the thickness of coatings and getting a depth composition profile. Some properties such as UV-absorption and barrier effect are highlighted using a UV-visible spectrometer and electrochemical impedance spectroscopy (EIS), respectively. The effect of ZnO concentration is also presented.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Applied Surface Science - Volume 327, 1 February 2015, Pages 379-388
Journal: Applied Surface Science - Volume 327, 1 February 2015, Pages 379-388
نویسندگان
A. Nicolay, A. Lanzutti, M. Poelman, B. Ruelle, L. Fedrizzi, Ph. Dubois, M.-G. Olivier,