Chemical shift tensor determination using magnetically oriented microcrystal array (MOMA): 13C solid-state CP NMR without MAS

► A microcrystalline powder was converted to a magnetically oriented microcrystal array. ► The chemical shift anisotropy was determined using 13C solid-state CP NMR without MAS. ► The principal values and axes showed good agreement with those of a single crystal. ► Chemical shift tensor is determined from a magnetically oriented microcrystal array.