کد مقاله کد نشریه سال انتشار مقاله انگلیسی نسخه تمام متن
5407185 1393206 2008 8 صفحه PDF دانلود رایگان
عنوان انگلیسی مقاله ISI
A simple, small and low cost permanent magnet design to produce homogeneous magnetic fields
موضوعات مرتبط
مهندسی و علوم پایه شیمی شیمی تئوریک و عملی
پیش نمایش صفحه اول مقاله
A simple, small and low cost permanent magnet design to produce homogeneous magnetic fields
چکیده انگلیسی
A new portable, pocket-size NMR probe based on a novel permanent magnet arrangement is presented. It is based on a Halbach-type magnet design which mimics the field of a spherical dipole by using cylindrical bar and ring magnets. The magnet system is made up of only three individual magnets, and most field calculations and optimisations can be performed analytically. A prototype system has been built using a set of small, off the shelf commercially available permanent magnets. Proton linewidths of 50 ppm FWHM could be achieved at a field strength of 1 T. Calculations show that with custom-sized permanent magnets, linewidths of less than 1 ppm can be achieved over sample volumes of up to 1 mm3, which would in theory enable chemical shift resolved proton spectroscopy on mass-limited samples. But even with the achieved linewidth of 50 ppm, this can be a useful portable sensor for small amounts of liquid samples with restricted molecular mobility, like gels, polymers or high viscosity liquids.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Journal of Magnetic Resonance - Volume 192, Issue 1, May 2008, Pages 131-138
نویسندگان
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