کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
7640224 | 1494853 | 2018 | 19 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
High throughput screening of phenolic constituents in a complex sample matrix using post-column derivatisations employing reaction flow HPLC columns
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کلمات کلیدی
موضوعات مرتبط
مهندسی و علوم پایه
شیمی
شیمی آنالیزی یا شیمی تجزیه
پیش نمایش صفحه اول مقاله
![عکس صفحه اول مقاله: High throughput screening of phenolic constituents in a complex sample matrix using post-column derivatisations employing reaction flow HPLC columns High throughput screening of phenolic constituents in a complex sample matrix using post-column derivatisations employing reaction flow HPLC columns](/preview/png/7640224.png)
چکیده انگلیسی
This communication is the first to demonstrate the high throughput power of a 30â¯mm in length reaction flow (RF) column to conduct a targeted analysis of phenolics in a complex sample matrix (tea) utilising post-column derivatisation (PCD). Sensitivity, speed and efficiency could be tuned via the selection of the RF column separation flow rate. RF-PCD compared to conventional PCD approach with a 100â¯Î¼L loop resulted in a gain of up to 150% in sensitivity. The reaction loop volumes employed in conventional PCD approaches will always be the limitation for compatibility with low dispersion chromatography systems and/or columns.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Microchemical Journal - Volume 141, September 2018, Pages 253-257
Journal: Microchemical Journal - Volume 141, September 2018, Pages 253-257
نویسندگان
Andrew Jones, AgustÃn Acquaviva, Gary R. Dennis, R. Andrew Shalliker, Arianne Soliven,