کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
7897552 | 1510118 | 2017 | 8 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Synthesis of highly disperse tetragonal BaTiO3 nanoparticles with core-shell by a hydrothermal method
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کلمات کلیدی
موضوعات مرتبط
مهندسی و علوم پایه
مهندسی مواد
سرامیک و کامپوزیت
پیش نمایش صفحه اول مقاله
چکیده انگلیسی
In order to synthesize of high-dispersion and tetragonal BaTiO3 (BT) nanoparticle, a hydrothermal method is used in a mixture of chloride metal sources and KOH with polyvinylpyrrolidone (PVP). The properties of BT-PVPs prepared by different reaction temperature and time are investigated via XRD, FE-SEM, DLS, FT-IR, and TEM to clarify the changes of the crystal phase, dispersion, and particle structure. The reaction is finished at 230 °C for 24 h and the critical reaction condition for that the crystal phase of the obtained BT particle changed from the cubic to the tetragonal is found to be 190 °C fixed in reaction time 24 h, and 9 h. During reaction the PVP on the BT surface decomposed to different form, and the PVP plays the role of dispersant in aqueous solution. By the hydrothermal condition of 230 °C for 24 h almost monodisperse BT-PVP with sizes of 83 nm and tetragonality (c/a) of 1.0062 were synthesized. The structure of nanoparticle, core (BT)-shell (PVP) was investigated by FT-IR and direct observed by TEM and the mechanism of particle growth and dispersion was discussed.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Journal of Asian Ceramic Societies - Volume 5, Issue 4, December 2017, Pages 444-451
Journal: Journal of Asian Ceramic Societies - Volume 5, Issue 4, December 2017, Pages 444-451
نویسندگان
Jinhui Li, Koji Inukai, Akihiro Tsuruta, Yosuke Takahashi, Woosuck Shin,