کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
7920029 | 1511486 | 2018 | 5 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Rapid synthesis of highly pure Nb2AlC using the spark plasma sintering technique
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کلمات کلیدی
موضوعات مرتبط
مهندسی و علوم پایه
مهندسی مواد
مواد الکترونیکی، نوری و مغناطیسی
پیش نمایش صفحه اول مقاله
چکیده انگلیسی
In this work, highly pure Nb2AlC was successfully synthesized using the spark plasma sintering (SPS) technique with Nb, NbC and black carbon as raw materials at 1450â¯Â°C and 30â¯MPa for 8â¯min. The obtained Nb2AlC grain shows a characteristic layered structure. More interestingly, the obtained Nb2AlC exhibits good electrical, thermal and mechanical properties. The coefficient of thermal expansion is 9.0â¯Ãâ¯10â6â¯Kâ1 from room temperature to 1200â¯Â°C. The electrical conductivity reaches 1.3â¯Ãâ¯106â¯Sâ¯m-1â¯at 500â¯Â°C, indicating excellent high-temperature conductivity. The Vickers hardness and flexural strength are 4.0â¯GPa and 440â¯Â±â¯10â¯MPa, respectively. Importantly, fracture toughness of the obtained Nb2AlC material reaches 7.8â¯Â±â¯0.2â¯MPaâ¯m1/2, which is higher than that of other previously studied MAX materials. Therefore, SPS is a very effective method to fabricate Nb2AlC materials and can also be used to prepare other MAX materials.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Journal of Physics and Chemistry of Solids - Volume 120, September 2018, Pages 218-222
Journal: Journal of Physics and Chemistry of Solids - Volume 120, September 2018, Pages 218-222
نویسندگان
Weibing Zhou, Kang Li, Jiaoqun Zhu, Shouqin Tian,