کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
8043276 | 1518723 | 2013 | 6 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Optimization of Sealed Tube Graphitization Method for Environmental C-14 Studies Using MICADAS
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موضوعات مرتبط
مهندسی و علوم پایه
مهندسی مواد
سطوح، پوششها و فیلمها
پیش نمایش صفحه اول مقاله
چکیده انگلیسی
The original sealed tube zinc reduction graphitization process was first developed for rapid low-precision measurements of biomedical tracer samples and later also applied for high precision measurements of not too old samples. In this study we tested the MICADAS (mini radiocarbon dating system [1]) radiocarbon measurements of targets prepared by sealed tube graphitization process. We found the optimal iron catalyst and reagents (TiH2 and Zn) amount whereby we can reach a relatively low background level, and minimized the overall δ13C fractionation during the graphitization. Repeated measurements of normalization standards and real samples with known 14C activities were very well reproduced. Finally, we demonstrated the applicability of the sealed tube graphitization on real environmental samples covering a wide range of 14C concentrations.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms - Volume 294, January 2013, Pages 270-275
Journal: Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms - Volume 294, January 2013, Pages 270-275
نویسندگان
László Rinyu, Mihály Molnár, István Major, Tamás Nagy, Mihály Veres, Ádám Kimák, Lukas Wacker, Hans-Arno Synal,