کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
830807 | 1470361 | 2012 | 11 صفحه PDF | دانلود رایگان |
In the current study, we investigated the effect of braze filler particle size and various processing parameters on vacuum diffusion brazing of thin foils of 3003 Al using a Ag nanoparticle (AgNPs) interlayer. All samples were brazed at 550 °C and 570 °C at heating rates of 5 °C/min and 25 °C/min under a pressure of 1 MPa. Differential scanning calorimetric results, involving 5 nm AgNPs, showed significant reduction in phase transformation temperature. Microstructures of brazed cross-sections revealed that nanoparticles aid formation of the joint at temperatures below the Al–Ag eutectic temperature of 567 °C. X-ray diffraction analysis of the interface showed the presence of δ-phase (Ag2Al) and μ-phase (Ag3Al). This was confirmed with energy dispersive spectroscopic analysis. A tensile strength of 69.7 MPa was achieved for a sample brazed at 570 °C with an interlayer of approximately 7 μm in thickness.
► 5 nm AgNPs showed size dependent melting behavior.
► 3003 Al alloy was brazed well below the Al–Ag eutectic (567 °C) temperature.
► Heating rate influenced the microstructural/phase changes at the bond interface.
► A 7 μm Ag interlayer resulted in shear stress of 69.7 MPa when brazed at 570 °C.
► Diffusion zone of ∼25 μm (one side) is a potential candidate for precision joining.
Journal: Materials & Design (1980-2015) - Volume 36, April 2012, Pages 13–23