کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
9693986 | 1459636 | 2005 | 11 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Full deconvolution of the instrumental coefficients in scanning calorimeter of heat flux type
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موضوعات مرتبط
مهندسی و علوم پایه
مهندسی شیمی
جریان سیال و فرایندهای انتقال
پیش نمایش صفحه اول مقاله
چکیده انگلیسی
A new method of full deconvolution of the instrumental coefficients in scanning calorimeter of heat flux type has been proposed, including reasonable determination method of the thermal contact resistance between the sample pan and its stage. The determination utilizes the response of dynamic heat capacity obtained by temperature-modulated (T-M) mode of a commercial differential scanning calorimeter used as a single calorimeter. By taking into account of the contribution of heat exchange with purge gas, an extension of standard modeling has been proposed for the evaluation of the instrumental coefficients. An alternative method bypassing the full deconvolution is also proposed.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Thermochimica Acta - Volume 436, Issues 1â2, 1 October 2005, Pages 15-25
Journal: Thermochimica Acta - Volume 436, Issues 1â2, 1 October 2005, Pages 15-25
نویسندگان
Akihiko Toda, Masamichi Hikosaka,