کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
9783211 | 1511871 | 2005 | 5 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Decomposition of process control agent during mechanical milling and its influence on displacement reactions in the Al-TiO2 system
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کلمات کلیدی
موضوعات مرتبط
مهندسی و علوم پایه
مهندسی مواد
مواد الکترونیکی، نوری و مغناطیسی
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چکیده انگلیسی
The process control agent (PCA) stearic acid has been used to prevent excessive cold welding during mechanical milling of an Al-TiO2 powder mixture. Gradual decomposition of the stearic acid during high-energy ball milling caused contamination of the powder with carbon. The decomposition rate was found to be 3-4 times faster when 2.5 wt.% instead of 5 wt.% of PCA have been used. This resulted in a higher degree of powder contamination-in the early stages of milling-for a lower initial PCA addition. The degree of contamination with carbon can readily be estimated by thermogravimetry and by the size of an endothermic peak at 875 °C, due to a reaction between aluminium carbide and titanium aluminide, in the trace of differential scanning calorimetry experiments.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Materials Chemistry and Physics - Volume 89, Issues 2â3, 15 February 2005, Pages 362-366
Journal: Materials Chemistry and Physics - Volume 89, Issues 2â3, 15 February 2005, Pages 362-366
نویسندگان
S. Kleiner, F. Bertocco, F.A. Khalid, O. Beffort,