Keywords: DM; diabetes mellitus; LD50; lethal dose that killed 50% of the rats; bg; blood glucose; FBG; fasting blood glucose; To; 0Â h; TLC; thin layer chromatography; 1H NMR; proton nuclear magnetic resonance spectroscopy; 13C NMR; carbon-13 nuclear magnetic reso
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Recent advances in column coatings for capillary electrophoresis of proteins
Keywords: Capillary coating; Dynamic coating; Permanent coating; Nanomaterials; Protein separation; EOF; electroosmotic flow; CE; capillary electrophoresis; LC; liquid chromatography; BFS; bare fused silica; BGE; background electrolyte; SDS; sodium dodecyl sulfate;
Impact of ligands and media on the structure and properties of biological and biomimetic iron-sulfur clusters
Keywords: CoA; coenzyme A; Cys; cysteine; Fd; ferredoxin; HiPIP; high-potential iron sulfur protein; His; histidine; Asp; aspartate; Glu; glutamate; Ser; serine; NHE; normal hydrogen electrode; HMQC; heteronuclear multiple quantum correlated spectroscopy; NMR; nucl
Keywords: GH5; globular domain of chicken H5; GH1; globular domain of Drosophila linker histone H1; ITC; isothermal titration calorimetry; MTSL; [S-(2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-3-yl) methyl methanethiosulfonate]; HMQC; Heteronuclear Multiple-Quantum C
Keywords: COSY; correlation spectroscopy; DDW; double de-ionized water; GSH; glutathione; HESI; heated electro spray ionization; HMBC; heteronuclear multiple-bond correlation spectroscopy; HMQC; heteronuclear multiple-quantum correlation spectroscopy; LOD; limit of
Improving reliability of chemometric models for authentication of species origin of heparin by switching from 1D to 2D NMR experiments
Keywords: NMR spectroscopy; HMQC; DOSY; Heparin; Animal origin; Classification;
Arylated gymnemic acids from Gymnema sylvestre R.Br. as potential α-glucosidase inhibitors
Keywords: COSY; correlation spectroscopy; DAGA; deacyl gymnemic acid; DEPT; distortionless enhancement by polarization transfer; DMSO; dimethyl sulfoxide; FTIR; fourier transform infra red; HRES-MS; high resolution electrospray mass spectrometry; MPLC; medium press
Mechanistic analyses of the suppression of amyloid β42 aggregation by apomorphine
Keywords: Aβ; amyloid β-protein; AD; Alzheimer's disease; HFIP; 1,1,1,3,3,3,-hexafluoroisopropyl alcohol; HMQC; heteronuclear multiple quantum coherence; HPLC; high performance liquid chromatography; LC-MS; liquid chromatography-mass spectrometry; LC/Q Tof-MS
Immunomodulatory, hemolytic and cytotoxic activity potentials of triterpenoid saponins from eight Cephalaria species
Keywords: Cytotoxic activity; Hemolytic activity; Immunomodulatory activity; Cephalaria; Caprifoliaceae; Triterpene saponin; HeLa; Human Cervix Adenocarcinoma; A549; Human Lung Adenocarcinoma; HEK293; Human Embryonic Kidney Cells; MTT; 3-(4,5-Dimethylthiazol-2-yl)-
Suppressive effects of Vochysia divergens aqueous leaf extract and its 5-methoxyflavone on murine macrophages and lymphocytes
Keywords: ConA; concanavalin A; COSY; correlation spectroscopy; COX-2; cyclooxygenase-2; CyA; cyclosporin A; DAB; diaminobenzidine; DMEM-F12; Dulbecco's Modified Eagle Medium- nutrient mixture F-12; DMSO; dimethyl sulfoxide; DPPH; 1,1-diphenyl- 2-picrylhydrazyl; FA
The O-β-linked N-acetylglucosaminylation of the Lamin B receptor and its impact on DNA binding and phosphorylation
Keywords: ETD/ECD MS; Electron Transfer Dissociation/Electron Capture Dissociation mass spectrometry; HILIC; hydrophilic interaction liquid chromatography; HMQC; heteronuclear multiple quantum correlation; HSQC; heteronuclear single quantum correlation; IPTG; isopr
Study on production enhancement of validamycin A using online capacitance measurement coupled with 1H NMR spectroscopy analysis in a plant-scale bioreactor
Keywords: NMR; nuclear magnetic resonance; GC; gas chromatography; MS; mass spectrometry; DCW; dry cell weight; HPLC; high-performance liquid chromatography; OUR; oxygen uptake rate; CER; carbon dioxide expiration rate; vvm; air volume/culture volume/min; HSQC; het
Inhibitory effects of (+)-spectaline and iso-6-spectaline from Senna spectabilis on the growth and ultrastructure of human-infective species Trypanosoma brucei rhodesiense bloodstream form
Keywords: Senna spectabilis; Piperidine alkaloids; (+)-spectaline; Iso-6-spectaline; Tyrpanosoma brucei rhodesiense; Autophagy; HAT; human African trypanosomiasis; DNDi; Drugs for Neglected Diseases initiative; IC50; half maximal inhibitory concentration; PCD; prog
Novel nor-monoterpenoid indole alkaloids inhibiting glioma stem cells from fruits of Alstonia scholaris
Keywords: Glioma stem cells; Antitumor activity; Alstonia scholaris; Nor-monoterpenoid indole alkaloids; GSC-3#; GSC-12# and GSC-18#, human glioma stem cells from clinical patients; HMBC; heteronuclear multiple bond correlation; HMQC; heteronuclear single quantum c
Thiocarbonyl-bound metallonitrosyl complexes with visible-light induced DNA cleavage and promising vasodilation activity
Keywords: bpy; 2,2-bipyridine; COSY; homonuclear correlation spectroscopy; cPTIO; 2-(4-carboxyphenyl)-4,4,5,5-tetramethylimidazoline-1-oxyl-3-oxide; HMBC; heteronuclear multiple quantum coherence; HMQC; heteronuclear multibond coherence; L-NAME; N-nitro-l-arginine
Isolation, purification, structural elucidation and antimicrobial activities of kocumarin, a novel antibiotic isolated from actinobacterium Kocuria marina CMG S2 associated with the brown seaweed Pelvetia canaliculata
Keywords: ATP; adenosine triphosphate; BB; broad-band; CEAE; crude ethyl acetate extract; CFU; colony-forming unit; CLSI; Clinical and Laboratory Standards Institute; COSY; correlation spectroscopy; DAPG; 2,4-diacetylphloroglucinol; DDH; DNA-DNA hybridization; DEPT
In silico investigation of cycloartane triterpene derivatives from Cimicifuga dahurica (Turcz.) Maxim. roots for the development of potent soluble epoxide hydrolase inhibitors
Keywords: AUDA; 12-(3-adamantan-1-yl-ureido)-dodecanoic acid; COSY; correlated spectroscopy; DHETs; dihydroxyeicosatrienoic acids; EETs; epoxyeicosatrienoic acids; HMBC; heteronuclear multiple bond connectivity; HMQC; heteronuclear multiple quantum coherence; NMR;
13C detected 15N13C coupling measurements at the natural isotopic abundance
Keywords: HCNMBC; HCNMQC; HMQC; 2D NMR; C-13 NMR; CN couplings; t1-noise;
3D correlation NMR spectrum between three distinct heteronuclei for the characterization of inorganic samples: Application on sodium alumino-phosphate materials
Keywords: 3D; INEPT; HMQC; Alumino-phosphate; Close Larmor frequencies;
Purification and characterization of the colicin A immunity protein in detergent micelles
Keywords: BS3; bis(sulfosuccinimidyl)suberate; C12E8; dodecyl octaethylene glycol ether; C12E9; dodecyl nonaethylene glycol ether; CD; circular dichroism; Cholate; 3α,7α,12α-trihydroxy-5β-cholan-24-oic acid, monosodium salt; CHAPS; 3-[(3-cholamidopropyl)-dimeth
Investigating the cytotoxicity of platinum(II) complexes incorporating bidentate pyridyl-1,2,3-triazole “click” ligands
Keywords: 2pq; 2-(2-pyridyl)quinoxaline; bnpytri; 2-(1-benzyl-1H-1,2,3-triazol-4-yl)pyridine; bpy; 2,2â²-bipyridine; dach; diaminocyclohexane; DMEM; Dulbecco's modified Eagle's medium; dpq; dipyrido[3,2-f:2â²,3â²-h]quinoxaline; HMQC; heteronuclear multiple quant
Antitumor lignanamides from the aerial parts of Corydalis saxicola
Keywords: Corydalis saxicola; Lignanamides; Corydalisin; Gastric cancer cells; Antiproliferative activities; DMSO; dimethyl sulfoxide; HMBC; heteronuclear multiple bond correlation; HMQC; heteronuclear single quantum coherence; ROESY; rotating frame Overhauser effe
Role of the Ï54 Activator Interacting Domain in Bacterial Transcription Initiation
Keywords: RNAP; RNA polymerase; DBD; DNA binding domain; NtrC1C; NtrC1 central domain construct; AID; activator interacting domain; CBD; core binding domain; A.a.; Aquifex aeolicus; E.c.; Escherichia coli; HSQC; heteronuclear single quantum coherence; HMQC; heteron
NMR spectroscopy with compact instruments
Keywords: Compact NMR; NMR spectroscopy; Product control; Reaction monitoring; 2D NMR; 1D; one-dimensional; 2D; two-dimensional; CDCl3; deuterated chloroform; COSY; correlation spectroscopy; DEPT; distortion-less enhancement by polarization transfer; EO; ethylene o
Studies of minute quantities of natural abundance molecules using 2D heteronuclear correlation spectroscopy under 100Â kHz MAS
Keywords: Ultrafast MAS; Indirect detection; HSQC; HMQC; Mesoporous silica nanoparticles;
Identification of cytotoxic and anti-inflammatory constituents from the bark of Toxicodendron vernicifluum (Stokes) F.A. Barkley
Keywords: (+)-(2S,3R)-Fustin (PubChem CID: 72282); (+)-Epitaxifolin (PubChem CID: 443758); Sulfuretin (PubChem CID: 5281295); Butein (PubChem CID: 5281222); Fisetin (PubChem CID: 5281614); Doxorubicin (PubChem CID: 31703); NG-monomethyl-l-arginine (PubChem CID: 135
Novel adducts from the reaction of 1-chloro-3-buten-2-one with 2â²-deoxyguanosine. Structural characterization and potential as tools to investigate 1,3-butadiene carcinogenicity
Keywords: ADH; alcohol dehydrogenase; BD; 1,3-butadiene; CBO; 1-chloro-3-buten-2-one; CHB; 1-chloro-2-hydroxy-butene; COSY; correlation spectroscopy; dG; 2â²-deoxyguanosine; DMSO-d6; hexadeuterodimethyl sulfoxide; ESI; electrospray ionization; HMBC; heteronuclear
Expression in yeast, new substrates, and construction of a first 3D model of human orphan cytochrome P450 2U1: Interpretation of substrate hydroxylation regioselectivity from docking studies
Keywords: AA; arachidonic acid; a.m.u.; atomic mass unit; a.u.; arbitrary units; CYP; cytochrome P450; Deb; debrisoquine; 1- 3-, 4-, 5-, 6-, 7- and 8-OH-Deb; 1-, 3-, 4-, 5-, 6-, 7-, and 8-hydroxy-debrisoquine, respectively; N-OH-Deb; N-hydroxy-debrisoquine; Deb-ure
Post-HTS case report and structural alert: Promiscuous 4-aroyl-1,5-disubstituted-3-hydroxy-2H-pyrrol-2-one actives verified by ALARM NMR
Keywords: acetyl-CoA; acetyl coenzyme A; ALARM NMR; a La assay to detect reactive molecules by nuclear magnetic resonance; Asf1; anti-silencing function 1; AZ; AstraZeneca; BME; β-mercaptoethanol; BSA; bovine serum albumin; CoA; coenzyme A; CPM; N-[4-(7-diethylami
NMR-based characterization of a novel yellow chlorophyll catabolite, Ed-YCC, isolated from Egeria densa
Keywords: ACN; acetonitrile; DPT; distortionless enhancement by polarization transfer; COSY; correlation spectroscopy; ESI; electrospray ionization; HMBC; heteronuclear multiple bond correlation; HMQC; heteronuclear multiple quantum coherence; HPLC; high-performanc
4-Methylthio-butanyl derivatives from the seeds of Raphanus sativus and their biological evaluation on anti-inflammatory and antitumor activities
Keywords: NMR; nuclear magnetic resonance; SRB; sulforhodamine B; NO; nitric oxide; LPS; lipopolysaccharide; IR; infrared; UV; ultraviolet; HR; high resolution; ESI; electrospray ionization; MS; mass spectrometry; COSY; correlation spectroscopy; HMQC; heteronuclear
Phenolic derivatives from the rhizomes of Dioscorea nipponica and their anti-neuroinflammatory and neuroprotective activities
Keywords: NMR; nuclear magnetic resonance; NO; nitric oxide; LPS; lipopolysaccharide; UV; ultraviolet; IR; infrared; HR; high resolution; FAB; fast atom bombardment; MS; mass spectrometry; COSY; correlation spectroscopy; HMQC; heteronuclear multiple quantum coheren
De novo biosynthesis of linoleic acid and its conversion to the hydrocarbon (Z,Z)-6,9-heptadecadiene in the astigmatid mite, Carpoglyphus lactis: Incorporation experiments with 13C-labeled glucose
Keywords: De novo biosynthesis; Linoleic acid; Essential fatty acid; (Z,Z)-6,9-heptadecadiene; Carpoglyphus lactis; Astigmata; FAs; fatty acids; FAMEs; fatty acid methyl esters; GC-MS; gas chromatography-mass spectrometry; LA; linoleic acid; LAME; linoleic acid
Improving the resolution in proton-detected through-space heteronuclear multiple quantum correlation NMR spectroscopy
Keywords: Solid state NMR; Indirect detection; Proton decoupling; HMQC; 14N;
Solution NMR determination of hydrogen bonding and base pairing between the glyQS T box riboswitch Specifier domain and the anticodon loop of tRNAGly
Keywords: NOESY; nuclear Overhauser effect spectroscopy; 2D; two dimensional; HMQC; heteronuclear multiple quantum coherence; NH; imino; CW; continuous wave; SD; specifier domain; Heteronuclear; U-turn; tRNA; Transcription regulation; Riboswitch; Antitermination; D
Proton-nitrogen-14 overtone two-dimensional correlation NMR spectroscopy of solid-sample at very fast magic angle sample spinning
Keywords: Solid-state NMR; 14N overtone; Very fast MAS; HMQC; 0.75Â mm MAS;
An in-cell NMR study of monitoring stress-induced increase of cytosolic Ca2+ concentration in HeLa cells
Keywords: HMQC; heteronuclear multiple quantum coherence; HSQC; heteronuclear single quantum coherence; In-cell NMR; HeLa cells; Cytosolic Ca2+ concentration; Calbindin D9k;
“Perfect Echo” HMQC: Sensitivity and resolution enhancement by broadband homonuclear decoupling
Keywords: Perfect echo; HMQC; Broadband homonuclear decoupling; J-Multiplets; J-Refocusing;
Is aristolochic acid nephropathy a widespread problem in developing countries?
Keywords: A; alstonine; AA; aristolochic acid; AAA; aristolochic acid analogue; AAN; aristolochic acid nephropathy; AL; aristolactam; BA; benzoic acid; BEN; Balkan endemic nephropathy; COSY; correlation spectroscopy; CP; commercial product; D2O; deuterated water; E
Fluorine detected 2D NMR experiments for the practical determination of size and sign of homonuclear F-F and heteronuclear C-F multiple bond J-coupling constants in multiple fluorinated compounds
Keywords: Fluorine NMR; Site-selective; XLOC; HMQC; Heteronuclear E.COSY; Coupling sign; Perfluorinated vinyl alkyl ether;
Heteronuclear NMR provides an accurate assessment of therapeutic insulin's quality
Keywords: SOFAST; band-selective optimized-flip-angle short-transient; HMQC; heteronuclear multiple quantum coherence; HSQC; heteronuclear single quantum correlation; EMEA; European Medicine Agency; SOFAST NMR; Insulin; Lispro; Biodrug; Biosimilar;
Synthesis, spectroscopic characterization, X-ray structure and DFT studies on 2,6-bis(1-benzyl-1H-benzo[d]imidazol-2-yl)pyridine
Keywords: X-ray structure determination; IR and NMR spectroscopy; HMQC; DFT calculations; Molecular electrostatic potential (MEP); Non-linear optical properties
Determination of size and sign of hetero-nuclear coupling constants from 2D 19F-13C correlation spectra
Keywords: NMR; Fluorine; HSQC; HMQC; HMBC; Decoupling; Coupling sign;
Lignan constituents of Tilia amurensis and their biological evaluation on antitumor and anti-inflammatory activities
Keywords: NMR; nuclear magnetic resonance; HRMS; high resolution mass spectrometry; CD; circular dichroism; IC50; inhibitory concentration; NO; nitric oxide; ESI; electrospray ionization; COSY; correlation spectroscopy; HMQC; heteronuclear multiple quantum coherenc
Gum ghatti: A promising polysaccharide for pharmaceutical applications
Keywords: GRAS; generally recognized as safe; 13C NMR; carbon 13 nuclear magnetic resonance; 2D NMR; two-dimensional nuclear magnetic resonance; COSY; correlation spectroscopy; TOCSY; total correlation spectroscopy; HMQC; heteronuclear multiple-quantum correlation;
Practical choice of 1H-1H decoupling schemes in through-bond 1H-{X} HMQC experiments at ultra-fast MAS
Keywords: Solid-state NMR; 1H; Very fast MAS; 1Â mm MAS; HMQC; CRAMPS;
Structural characterization of an acidic polysaccharide from Dalbergia sissoo Roxb. leaves
Keywords: Dalbergia sissoo; Polysaccharide; Structure; HMQC; Glucuronic acid;
Biological activities of Pseudevernia furfuracea (L.) Zopf extracts and isolation of the active compounds
Keywords: ASA; Acetylsalicylic acid; BuOH; Butanol; CC; Column chromatography; DCM; Dichloromethane; DPPH; 2,2-diphenyl-1-picrylhydrazyl; EtOAc; Ethyl acetate; HMBC; Heteronuclear Multiple Bond Correlation; HMQC; Heteronuclear Multiple-Quantum Correlation; MeOH; Me
Immunomodulatory active compounds from Tinospora cordifolia
Keywords: DEPT; distortionless enhancement by polarization transfer; HMQC; heteronuclear multiple quantum correlation; HMBC; heteronuclear multiple mond correlation; ESI-QTOF-MS; electrospray ionization-quadrupole time of flight-mass spectrum; MEM; minimum essentia
Structural data on a bacterial exopolysaccharide produced by a deep-sea Alteromonas macleodii strain
Keywords: EPS; exopolysaccharide; GLC; gas-liquid chromatography; COSY; correlation spectroscopy; TOCSY; total correlation spectroscopy; HMBC; heteronuclear multiple bond correlation; HMQC; heteronuclear multiple bond quantum coherence; amu; atomic mass units; Ba