Analysis of the spatial distribution of geochemical signatures for the identification of prehistoric settlement patterns in ADE and TMA sites in the lower Amazon Basin

The Archeological Dark Earth (ADE) and Terra Mulata (TMA) anthrosols found at Juruti, on the lower Amazon River, extend over a wide area located within the local ferralsol domain. The ADE soils are dark in color and contain large quantities of fragmented ceramics, while the TMA soils are also relatively dark, but lack ceramics. Multi-element chemical analyses of soil samples of ADE and TMA from the A2 horizon (depths of 10–20 cm) indicated that the ADE soils are characterized by higher concentrations of P2O5, CaO, K2O, MgO, Cu, Mn, and Zn, while the TMAs have median levels of these compounds, and the ferralsols have much lower concentrations. These chemical elements make up the geochemical signature of these anthrosols, whereas Al2O3, Fe2O3, TiO2, Cr, Sr, La, Li, Ni, Pb, V, Y, and Zr characterize the geochemical signature of the ferralsols, which was identified partially in the ADEs and TMAs. The isoline maps of these two geochemical associations permitted the delimitation of the different areas and the identification of the ADEs as sites of long-term human occupancy, and the TMA as an area of temporary occupation associated with agricultural activities. Seven villages were delimited within the study area, and were separated by corridors of ferralsols. These settlements were established on the riverbank, with the more temporary cultivated areas behind them, running almost parallel to the river. The identification of functional patterns based on geochemical associations, the abundance of ceramic material, and concentrations of organic matter, indicated that an area of more than 350 ha was occupied.

► The soils Archeological Dark Earth (ADE) and Terra Mulata (TMA) are typical of the Amazon region.
► The concentrations of P2O5 and CaO in the ADE reflect the presence of fragments of bone and amorphous phosphates.
► Geochemical association delimit an ample area to the rear of the seven villages.
► The chemical composition of the ADE and TMAs indicates their derivation from Ferralsols.