کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
10624099 | 989583 | 2016 | 6 صفحه PDF | دانلود رایگان |
عنوان انگلیسی مقاله ISI
Synthesis and spark plasma sintering of the α-Si3N4 nanopowder
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کلمات کلیدی
موضوعات مرتبط
مهندسی و علوم پایه
مهندسی مواد
سرامیک و کامپوزیت
پیش نمایش صفحه اول مقاله
چکیده انگلیسی
A two-step process (milling and then heat treatment) was used for the preparation of α-Si3N4 nanopowder. The influence of the milling time and heat treatment temperature as processing parameters were investigated on the formation of α-Si3N4. Silicon nitride ceramic was produced by spark plasma sintering at 1700 °C for 15 min, using MgSiN2 additive. The optimum sample was produced in a 30 h milling time, heat treatment at 1300 °C, and a 22 °C/min heating rate conditions. X-ray fluorescence analysis showed that the purity of the final product is above 98%. Nanoindentation hardness and Young's modulus of the SPS-ed sample were measured as 17±2.0 GPa and 290±11.0 GPa, respectively.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Ceramics International - Volume 42, Issue 13, October 2016, Pages 14867-14872
Journal: Ceramics International - Volume 42, Issue 13, October 2016, Pages 14867-14872
نویسندگان
Mohammad Khajelakzay, Saeed Reza Bakhshi, Gholam Hossein Borhani, Mazaher Ramazani,