کد مقاله کد نشریه سال انتشار مقاله انگلیسی نسخه تمام متن
10625496 989626 2014 20 صفحه PDF دانلود رایگان
عنوان انگلیسی مقاله ISI
Synthesis and characterization of ultrafine sub-micron Na-LTA zeolite particles prepared via hydrothermal template-free method
موضوعات مرتبط
مهندسی و علوم پایه مهندسی مواد سرامیک و کامپوزیت
پیش نمایش صفحه اول مقاله
Synthesis and characterization of ultrafine sub-micron Na-LTA zeolite particles prepared via hydrothermal template-free method
چکیده انگلیسی
Ultrafine sub-micron Na-LTA zeolite crystals ranging from 150 to 350 nm were synthesized without template via hydrothermal method. Aluminum iso-propoxide and colloidal silica were used as Al and Si sources, respectively, to synthesize the small and uniform zeolite crystals. Zeolite Na-LTA was synthesized hydrothermally from a gel formula of 1.0 Al2O3: 2.7 SiO2: 5.85 Na2O: 150H2O in molar basis. The crystallization conditions including synthesis time, and synthesis temperature were optimized to reduce the zeolite particle size. The final crystals were characterized by X-ray diffraction (XRD) and scanning electron microscopy (SEM). The results confirmed that synthesis temperature should be lowered for better control of the crystal growth. On the other hand, at low synthesis temperatures, synthesis time should be extended to acquire the high crystallinity. Ultrafine sub-micron Na-LTA zeolite crystals were synthesized at synthesis temperature of 60 °C and synthesis time of 11 h.
ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Ceramics International - Volume 40, Issue 8, Part A, September 2014, Pages 12075-12080
نویسندگان
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