کد مقاله کد نشریه سال انتشار مقاله انگلیسی نسخه تمام متن
1191651 963575 2007 9 صفحه PDF دانلود رایگان
عنوان انگلیسی مقاله ISI
MIR spectroscopy and partial least-squares regression for determination of phospholipids in rapeseed oils at various stages of technological process
موضوعات مرتبط
مهندسی و علوم پایه شیمی شیمی آنالیزی یا شیمی تجزیه
پیش نمایش صفحه اول مقاله
MIR spectroscopy and partial least-squares regression for determination of phospholipids in rapeseed oils at various stages of technological process
چکیده انگلیسی

Fourier transform-mid infrared spectroscopy (FT-MIR) and partial least-square (PLS) regression were used for determination of phospholipids (PL) in rapeseed oils at various stages of technological process. The standard error of calibration (SEC) and the standard error of prediction (SEP) were calculated for evaluation of the calibration models. The chemometric calibration model was prepared in spectral region 1760–860 cm−1 for standard PL solutions (1.5–120 mg/mL). Obtained mean concentrations of PL in rapeseed oils at different stages of conventional technological operations varied from 22,710 to 224.6 mg/kg. Satisfactory values of precision (RSD = 0.23–0.73%) and accuracy (recovery – 96.1–101.9%), demonstrate the benefit of the proposed MIR-PLS method in the routine analysis of PL in vegetable oils.

ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Food Chemistry - Volume 105, Issue 3, 2007, Pages 1179–1187
نویسندگان
,