کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
---|---|---|---|---|
1269881 | 972465 | 2009 | 9 صفحه PDF | دانلود رایگان |
![عکس صفحه اول مقاله: Influence of the solvent on ultrasonically produced SbSI nanowires Influence of the solvent on ultrasonically produced SbSI nanowires](/preview/png/1269881.png)
The influence of the substitution of methanol in place of ethanol during the ultrasonic production of antimony sulfoiodide (SbSI) nanowires is presented. The new technology is faster and more efficient at temperatures greater than 314 K. The products were characterized by using techniques such as powder X-ray diffraction (XRD), scanning electron microscopy (SEM), energy dispersive X-ray analysis (EDXA), high-resolution transmission electron microscopy (HRTEM), selected area electron diffraction (SAED), optical diffuse reflection spectroscopy (DRS) and IR spectroscopy. The coexistence of Pna21 (ferroelectric) and Pnam (paraelectric) phases at 298 K was observed in the SbSI nanowires produced in methanol. The methanol decomposes during the sonication or due to the adsorption process on SbSI nanowires.
Journal: Ultrasonics Sonochemistry - Volume 16, Issue 4, April 2009, Pages 537–545