کد مقاله کد نشریه سال انتشار مقاله انگلیسی نسخه تمام متن
1297299 973841 2011 5 صفحه PDF دانلود رایگان
عنوان انگلیسی مقاله ISI
Influence of spray granulation on the properties of wet chemically synthesized Li1.3Ti1.7Al0.3(PO4)3 (LATP) powders
موضوعات مرتبط
مهندسی و علوم پایه شیمی الکتروشیمی
پیش نمایش صفحه اول مقاله
Influence of spray granulation on the properties of wet chemically synthesized Li1.3Ti1.7Al0.3(PO4)3 (LATP) powders
چکیده انگلیسی

Solid electrolyte materials Li1.3Al0.3Ti1.7(PO4)3 (NASICON, R-3c) were synthesized via novel acetate routes A (simple precipitate), A1 (spray-dried precipitate) and B (sol–gel synthesis) and their properties are compared. Spray-dried spherical granules show characteristic features as a result of their particular microstructure. Temperature dependent DC measurements provide an informative basis to discuss two different grain boundary ionic conduction mechanisms in these spray-dried granules.


► LATP materials were synthesized via novel acetate routes.
► Particle morphology can be adjusted via synthesis conditions and processing.
► Spray-drying offers an interesting way to increase total ionic conductivity σtot.
► Two grain boundary ionic conduction mechanisms in spherical granules are discussed.

ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Solid State Ionics - Volume 201, Issue 1, 19 October 2011, Pages 49–53
نویسندگان
, , ,