کد مقاله کد نشریه سال انتشار مقاله انگلیسی نسخه تمام متن
1340248 979727 2009 4 صفحه PDF دانلود رایگان
عنوان انگلیسی مقاله ISI
Synthesis and characterization of NiO nanoclusters via thermal decomposition
موضوعات مرتبط
مهندسی و علوم پایه شیمی شیمی معدنی
پیش نمایش صفحه اول مقاله
Synthesis and characterization of NiO nanoclusters via thermal decomposition
چکیده انگلیسی

Thermal decomposition process has been developed to synthesize nickel oxide (NiO) nanoclusters via the reaction between a new precursor, nickel oxalate [Ni(O4C2)(H2O)4] and oleylamine (C18H37N). The combination of triphenylphosphine (C18H15P) and C18H37N were added as surfactants to control the particle size. The products were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), Fourier transform infrared (FT-IR) spectroscopy, thermogravimetric analysis (TGA) and ultraviolet–visible (UV–Vis) spectroscopy. The synthesized NiO nanoclusters have a cubic structure with average size 2–10 nm.

Thermal decomposition process has been developed to synthesize nickel oxide (NiO) nanoclusters via the reaction between a new precursor, nickel oxalate [Ni(O4C2)(H2O)4] and oleylamine (C18H37N). The combinations of triphenylphosphine (C18H15P) and C18H37N were added as surfactants to control the particle size. The products were characterized different methods. The synthesized NiO nanoclusters have a cubic structure with average size 2–10 nm.Figure optionsDownload as PowerPoint slide

ناشر
Database: Elsevier - ScienceDirect (ساینس دایرکت)
Journal: Polyhedron - Volume 28, Issue 6, 23 April 2009, Pages 1111–1114
نویسندگان
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