کد مقاله | کد نشریه | سال انتشار | مقاله انگلیسی | نسخه تمام متن |
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1461138 | 989616 | 2014 | 7 صفحه PDF | دانلود رایگان |
![عکس صفحه اول مقاله: Microwave-assisted preparation of submicron-sized FeTiO3 powders Microwave-assisted preparation of submicron-sized FeTiO3 powders](/preview/png/1461138.png)
FeTiO3 powders were prepared from (Fe+Ti) mixed carbonate precursor by the microwave-assisted calcination method. The thermal analysis of the precursor was conducted by TG/DSC. It is demonstrated that the calcination process can be divided into three different stages: the removal of water, the decomposition of precursor and the formation of FeTiO3. A variety of techniques, such as XRD, FT-IR, SEM and EDS were utilized to characterize the samples. The results indicated that FeTiO3 powders can be prepared by microwave-assisted calcination for 20 min at 450 °C, while those cannot be obtained by conventional one until reaction time exceeds 120 min at 600 °C. The FeTiO3 powders prepared by microwave-assisted calcination are nearly spherical with limited aggregation and have a mean particle size of 400–500 nm.
Journal: Ceramics International - Volume 40, Issue 5, June 2014, Pages 6799–6805